Information card for entry 1563930

Structure parameters

• Formula: C42 H68 Cl14 P4 Rh2
• Calculated formula: C42 H68 Cl14 P4 Rh2
• Title of publication: Oxidative addition of methylene chloride to Me-DuPhos complexes of palladium and rhodium
• Authors of publication: Scheetz, Perry M.; Blank, Natalia F.; Gibbons, Sarah K.; Glueck, David S.; Rheingold, Arnold L.
• Journal of publication: Inorganica Chimica Acta
• Year of publication: 2018
• Journal volume: 483
• Pages of publication: 111 - 115
• a: 12.6298 ± 0.0006 Å
• b: 20.0689 ± 0.0009 Å
• c: 22.7254 ± 0.0009 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 5760.1 ± 0.4 ų
• Cell temperature: 100 K
• Ambient diffraction temperature: 100 K
• Number of distinct elements: 5
• Space group number: 19
• Hermann-Mauguin space group symbol: P 21 21 21
• Hall space group symbol: P 2ac 2ab
• Residual factor for all reflections: 0.0946
• Residual factor for significantly intense reflections: 0.0622
• Weighted residual factors for significantly intense reflections: 0.1226
• Weighted residual factors for all reflections included in the refinement: 0.1376
• Goodness-of-fit parameter for all reflections included in the refinement: 1.036
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No