Information card for entry 1564337

Structure parameters

• Formula: C14 H31 B O2 Si
• Calculated formula: C14 H31 B O2 Si
• Title of publication: Synthesis of hydrosilylboronates via the monoborylation of a dihydrosilane Si‒H bond and their application for the generation of dialkylhydrosilyl anions
• Authors of publication: Takeuchi, Takumi; Shishido, Ryosuke; Kubota, Koji; Ito, Hajime
• Journal of publication: Chemical Science
• Year of publication: 2021
• a: 12.7304 ± 0.0006 Å
• b: 14.6636 ± 0.0006 Å
• c: 9.7331 ± 0.0004 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 1816.91 ± 0.14 ų
• Cell temperature: 173 K
• Ambient diffraction temperature: 173 K
• Number of distinct elements: 5
• Space group number: 62
• Hermann-Mauguin space group symbol: P n m a
• Hall space group symbol: -P 2ac 2n
• Residual factor for all reflections: 0.0948
• Residual factor for significantly intense reflections: 0.0772
• Weighted residual factors for significantly intense reflections: 0.2346
• Weighted residual factors for all reflections included in the refinement: 0.2568
• Goodness-of-fit parameter for all reflections included in the refinement: 1.043
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No