Information card for entry 1564466

Structure parameters

• Formula: Co3 H61 Na14 O99.5 P2 W18
• Calculated formula: Co3 Na14 O99.492 P2 W18
• Title of publication: Synthesis, structure, and properties of the multinuclear cobalt core POM Na14[Co3O(H2O)(A-α-PW9O34)2]·~29.5H2O
• Authors of publication: Rehan, Kanwar; Asma, Maliha; McMillen, Colin D.; Sokolov, Andrei; Sohail, Manzar; Sher, Muhammad; Shafique, Munib Ahmed; Bukhari, Naheed; Tirmizi, Syed Ahmad
• Journal of publication: Inorganica Chimica Acta
• Year of publication: 2020
• Journal volume: 509
• Pages of publication: 119690
• a: 12.2204 ± 0.0008 Å
• b: 16.7035 ± 0.0011 Å
• c: 23.3466 ± 0.0016 Å
• α: 78.448 ± 0.002°
• β: 80.551 ± 0.002°
• γ: 78.448 ± 0.002°
• Cell volume: 4536.1 ± 0.5 ų
• Cell temperature: 170 ± 2 K
• Ambient diffraction temperature: 170 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0355
• Residual factor for significantly intense reflections: 0.0282
• Weighted residual factors for significantly intense reflections: 0.0668
• Weighted residual factors for all reflections included in the refinement: 0.0701
• Goodness-of-fit parameter for all reflections included in the refinement: 1.051
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No