Information card for entry 1564826

Structure parameters

• Formula: C6 H40 N2 Na4 O30 P6 Pb2
• Calculated formula: C6 H40 N2 Na4 O30 P6 Pb2
• Title of publication: Chelate Complexes of Lead(II) with Nitrilotris(methylenephosphonic) Acid [Pb{5-NH(CH2PO3H)3}] and Na4[Pb2(H2O)2{3-N(CH2PO3)3H2}2] 10H2O: Synthesis, Structure, and Asymmetry of Lone 6s Pair
• Authors of publication: Somov, N.V.; Chausov, F.F.; Zakirova, R.M.; Reshetnikov, S.M.; Shishkin, A.S.; Shumilova, M.A.; Aleksandrov, V.A.; Petrov, V.G.
• Journal of publication: Crystallography Reports
• Year of publication: 2017
• Journal volume: 62
• Journal issue: 6
• Pages of publication: 857 - 867
• a: 10.8942 ± 0.0003 Å
• b: 13.1882 ± 0.0004 Å
• c: 14.0016 ± 0.0004 Å
• α: 65.885 ± 0.003°
• β: 82.401 ± 0.002°
• γ: 83.143 ± 0.002°
• Cell volume: 1815.23 ± 0.1 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0304
• Residual factor for significantly intense reflections: 0.0244
• Weighted residual factors for significantly intense reflections: 0.0512
• Weighted residual factors for all reflections included in the refinement: 0.0535
• Goodness-of-fit parameter for all reflections included in the refinement: 1.091
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No