#------------------------------------------------------------------------------
#$Date: 2021-11-05 00:15:24 +0100 (Fri 05 de Nov de 2021) $
#$Revision: 270309 $
#$URL: svn://www.crystallography.net/cod/cif/1/56/51/1565124.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_1565124
loop_
_publ_author_name
'Masson, Eric'
'Rabbani, Ramin'
'Saeedi, Sima'
'Nazimuddin, Md'
'Barbero, Hector'
'Kyritsakas, Nathalie'
'White, Travis A.'
_publ_section_title
;
 Enhanced photoreduction of water catalyzed by a cucurbit[8]uril-secured
 platinum dimer
;
_journal_name_full               'Chemical Science'
_journal_paper_doi               10.1039/D1SC03743A
_journal_year                    2021
_chemical_formula_moiety         'C48H48N32O16,2(C22H17ClN3Pt)+ solvent'
_chemical_formula_sum            'C92 H82 Cl2 N38 O16 Pt2'
_chemical_formula_weight         2437.03
_space_group_crystal_system      triclinic
_space_group_IT_number           2
_space_group_name_Hall           '-P 1'
_space_group_name_H-M_alt        'P -1'
_atom_sites_solution_hydrogens   geom
_audit_creation_method           SHELXL-2014/6
_audit_update_record
;
2021-07-06 deposited with the CCDC.	2021-11-04 downloaded from the CCDC.
;
_cell_angle_alpha                89.44
_cell_angle_beta                 82.949(4)
_cell_angle_gamma                89.97
_cell_formula_units_Z            4
_cell_length_a                   17.9543(13)
_cell_length_b                   20.7821(16)
_cell_length_c                   33.976(3)
_cell_measurement_reflns_used    9100
_cell_measurement_temperature    173(2)
_cell_measurement_theta_max      25.
_cell_measurement_theta_min      2.5
_cell_volume                     12580.9(17)
_computing_cell_refinement       'Bruker SAINT'
_computing_data_collection       'Bruker APEX2'
_computing_data_reduction        'Bruker SAINT'
_computing_molecular_graphics    'Bruker SHELXTL'
_computing_publication_material  'Bruker SHELXTL'
_computing_structure_refinement  'SHELXL-2014 (Sheldrick 2014)'
_computing_structure_solution    'SHELXS-97 (Sheldrick 2008)'
_diffrn_ambient_temperature      173(2)
_diffrn_measured_fraction_theta_full 0.963
_diffrn_measured_fraction_theta_max 0.906
_diffrn_measurement_device_type  'Bruker APEX-II CCD'
_diffrn_measurement_method       'φ and ω scans'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0581
_diffrn_reflns_av_unetI/netI     0.0519
_diffrn_reflns_Laue_measured_fraction_full 0.963
_diffrn_reflns_Laue_measured_fraction_max 0.906
_diffrn_reflns_limit_h_max       23
_diffrn_reflns_limit_h_min       -23
_diffrn_reflns_limit_k_max       25
_diffrn_reflns_limit_k_min       -24
_diffrn_reflns_limit_l_max       44
_diffrn_reflns_limit_l_min       -44
_diffrn_reflns_number            264585
_diffrn_reflns_point_group_measured_fraction_full 0.963
_diffrn_reflns_point_group_measured_fraction_max 0.906
_diffrn_reflns_theta_full        25.600
_diffrn_reflns_theta_max         27.600
_diffrn_reflns_theta_min         1.762
_exptl_absorpt_coefficient_mu    2.331
_exptl_absorpt_correction_T_max  0.821
_exptl_absorpt_correction_T_min  0.800
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details   sadabs
_exptl_crystal_colour            colorless
_exptl_crystal_density_diffrn    1.287
_exptl_crystal_density_meas      ?
_exptl_crystal_description       prism
_exptl_crystal_F_000             4872
_exptl_crystal_size_max          0.100
_exptl_crystal_size_mid          0.100
_exptl_crystal_size_min          0.090
_refine_diff_density_max         3.504
_refine_diff_density_min         -4.534
_refine_diff_density_rms         0.203
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.105
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     2633
_refine_ls_number_reflns         47500
_refine_ls_number_restraints     10
_refine_ls_restrained_S_all      1.105
_refine_ls_R_factor_all          0.1145
_refine_ls_R_factor_gt           0.1011
_refine_ls_shift/su_max          0.002
_refine_ls_shift/su_mean         0.058
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[σ²(Fo²)+(0.0699P)²+328.0372P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.2486
_refine_ls_wR_factor_ref         0.2554
_reflns_Friedel_coverage         0.000
_reflns_number_gt                39282
_reflns_number_total             47500
_reflns_threshold_expression     'I > 2σ(I)'
_cod_data_source_file            d1sc03743a2.cif
_cod_data_source_block           e4624n_a
_cod_depositor_comments
;
The following automatic conversions were performed:

data item '_exptl_crystal_density_meas' value 'none' was changed to
'?' -- the value is perceived as not measured.

Automatic conversion script
Id: cif_fix_values 7556 2019-12-06 15:28:31Z antanas 
;
_cod_original_cell_volume        12581.1(16)
_cod_database_code               1565124
_shelx_space_group_comment
;
The symmetry employed for this shelxl refinement is uniquely defined
by the following loop, which should always be used as a source of
symmetry information in preference to the above space-group names.
They are only intended as comments.
;
_shelx_estimated_absorpt_t_min   0.800
_shelx_estimated_absorpt_t_max   0.818
_shelxl_version_number           2014/6
loop_
_space_group_symop_operation_xyz
'x, y, z'
'-x, -y, -z'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_site_symmetry_order
_atom_site_calc_flag
_atom_site_refinement_flags_posn
_atom_site_refinement_flags_adp
_atom_site_refinement_flags_occupancy
_atom_site_disorder_assembly
_atom_site_disorder_group
O1 O 0.5124(6) 0.1879(5) 0.7403(3) 0.055(3) Uani 1 1 d . . . . .
C1 C 0.5474(8) 0.2286(7) 0.7541(4) 0.041(3) Uani 1 1 d . . . . .
N1 N 0.5861(6) 0.2224(6) 0.7872(3) 0.040(3) Uani 1 1 d . . . . .
N2 N 0.5588(7) 0.2906(6) 0.7396(3) 0.046(3) Uani 1 1 d . . . . .
C2 C 0.6286(8) 0.2794(8) 0.7929(4) 0.048(4) Uani 1 1 d . . . . .
H2 H 0.6834 0.2692 0.7909 0.058 Uiso 1 1 calc R U . . .
C3 C 0.6129(9) 0.3250(7) 0.7591(4) 0.048(4) Uani 1 1 d . . . . .
H3 H 0.6595 0.3344 0.7406 0.057 Uiso 1 1 calc R U . . .
N3 N 0.5852(6) 0.3818(6) 0.7804(3) 0.042(3) Uani 1 1 d . . . . .
N4 N 0.6057(7) 0.3146(6) 0.8279(3) 0.040(3) Uani 1 1 d . . . . .
C4 C 0.5877(9) 0.3760(9) 0.8190(5) 0.058(5) Uani 1 1 d . . . . .
O2 O 0.5683(7) 0.4189(5) 0.8444(3) 0.059(3) Uani 1 1 d . . . . .
C5 C 0.5403(10) 0.3081(8) 0.7000(4) 0.054(4) Uani 1 1 d . . . . .
H5A H 0.5873 0.3198 0.6831 0.065 Uiso 1 1 calc R U . . .
H5B H 0.5191 0.2698 0.6883 0.065 Uiso 1 1 calc R U . . .
C6 C 0.5800(8) 0.4437(7) 0.7597(4) 0.046(4) Uani 1 1 d . . . . .
H6A H 0.5805 0.4790 0.7790 0.056 Uiso 1 1 calc R U . . .
H6B H 0.6244 0.4490 0.7396 0.056 Uiso 1 1 calc R U . . .
C7 C 0.4243(9) 0.3521(7) 0.6809(4) 0.043(4) Uani 1 1 d . . . . .
O3 O 0.3989(7) 0.3016(5) 0.6693(3) 0.061(3) Uani 1 1 d . . . . .
N5 N 0.4889(8) 0.3596(6) 0.6994(3) 0.048(3) Uani 1 1 d . . . . .
N6 N 0.3956(6) 0.4121(6) 0.6744(3) 0.040(3) Uani 1 1 d . . . . .
C8 C 0.5080(8) 0.4257(7) 0.7007(4) 0.044(3) Uani 1 1 d . . . . .
H8 H 0.5555 0.4349 0.6830 0.052 Uiso 1 1 calc R U . . .
C9 C 0.4422(8) 0.4641(7) 0.6870(4) 0.042(3) Uani 1 1 d . . . . .
H9 H 0.4591 0.4949 0.6649 0.051 Uiso 1 1 calc R U . . .
N7 N 0.4106(6) 0.4964(6) 0.7223(3) 0.036(3) Uani 1 1 d . . . . .
N8 N 0.5130(6) 0.4487(6) 0.7404(3) 0.042(3) Uani 1 1 d . . . . .
C10 C 0.4544(8) 0.4925(7) 0.7518(4) 0.044(3) Uani 1 1 d . . . . .
O4 O 0.4485(6) 0.5208(6) 0.7828(3) 0.059(3) Uani 1 1 d . . . . .
C11 C 0.3348(7) 0.4251(7) 0.6514(3) 0.038(3) Uani 1 1 d . . . . .
H11A H 0.3511 0.4586 0.6312 0.045 Uiso 1 1 calc R U . . .
H11B H 0.3238 0.3855 0.6372 0.045 Uiso 1 1 calc R U . . .
C12 C 0.3623(8) 0.5526(7) 0.7200(4) 0.044(3) Uani 1 1 d . . . . .
H12A H 0.3675 0.5811 0.7426 0.053 Uiso 1 1 calc R U . . .
H12B H 0.3787 0.5769 0.6953 0.053 Uiso 1 1 calc R U . . .
C13 C 0.2008(8) 0.4154(7) 0.6750(4) 0.043(3) Uani 1 1 d . . . . .
O5 O 0.1961(7) 0.3607(5) 0.6612(4) 0.070(4) Uani 1 1 d . . . . .
N9 N 0.2691(6) 0.4456(6) 0.6741(3) 0.041(3) Uani 1 1 d . . . . .
N10 N 0.1441(6) 0.4532(6) 0.6888(3) 0.044(3) Uani 1 1 d . . . . .
C14 C 0.2563(7) 0.5144(6) 0.6844(4) 0.034(3) Uani 1 1 d . . . . .
H14 H 0.2731 0.5439 0.6616 0.041 Uiso 1 1 calc R U . . .
C15 C 0.1697(7) 0.5168(7) 0.6963(4) 0.040(3) Uani 1 1 d . . . . .
H15 H 0.1466 0.5491 0.6795 0.048 Uiso 1 1 calc R U . . .
N11 N 0.1613(6) 0.5367(5) 0.7361(3) 0.042(3) Uani 1 1 d . . . . .
N12 N 0.2843(6) 0.5344(5) 0.7206(3) 0.037(3) Uani 1 1 d . . . . .
C16 C 0.2293(8) 0.5489(6) 0.7493(3) 0.038(3) Uani 1 1 d . . . . .
O6 O 0.2383(6) 0.5718(5) 0.7818(3) 0.050(3) Uani 1 1 d . . . . .
C17 C 0.0688(8) 0.4371(8) 0.6860(4) 0.050(4) Uani 1 1 d . . . . .
H17A H 0.0677 0.3991 0.6687 0.060 Uiso 1 1 calc R U . . .
H17B H 0.0450 0.4733 0.6730 0.060 Uiso 1 1 calc R U . . .
C18 C 0.0906(8) 0.5581(6) 0.7574(4) 0.042(3) Uani 1 1 d . . . . .
H18A H 0.0638 0.5846 0.7392 0.050 Uiso 1 1 calc R U . . .
H18B H 0.1011 0.5857 0.7796 0.050 Uiso 1 1 calc R U . . .
C19 C 0.0009(7) 0.3618(7) 0.7353(4) 0.039(3) Uani 1 1 d . . . . .
O7 O 0.0186(6) 0.3138(5) 0.7173(3) 0.049(2) Uani 1 1 d . . . . .
N13 N 0.0246(7) 0.4231(6) 0.7236(3) 0.048(3) Uani 1 1 d . . . . .
N14 N -0.0445(6) 0.3676(6) 0.7707(3) 0.044(3) Uani 1 1 d . . . . .
C20 C -0.0098(8) 0.4720(7) 0.7495(4) 0.042(3) Uani 1 1 d . . . . .
H20 H -0.0394 0.5033 0.7351 0.050 Uiso 1 1 calc R U . . .
C21 C -0.0606(7) 0.4329(7) 0.7811(4) 0.045(4) Uani 1 1 d . . . . .
H21 H -0.1149 0.4431 0.7804 0.053 Uiso 1 1 calc R U . . .
N15 N -0.0346(7) 0.4533(5) 0.8188(3) 0.044(3) Uani 1 1 d . . . . .
N16 N 0.0419(6) 0.5050(6) 0.7731(3) 0.046(3) Uani 1 1 d . . . . .
C22 C 0.0208(7) 0.4965(7) 0.8133(4) 0.040(3) Uani 1 1 d . . . . .
O8 O 0.0480(5) 0.5262(5) 0.8391(2) 0.046(2) Uani 1 1 d . . . . .
C23 C -0.0871(11) 0.3134(8) 0.7876(4) 0.059(5) Uani 1 1 d . . . . .
H23A H -0.0778 0.2765 0.7695 0.071 Uiso 1 1 calc R U . . .
H23B H -0.1412 0.3241 0.7894 0.071 Uiso 1 1 calc R U . . .
C24 C -0.0826(9) 0.4418(7) 0.8566(4) 0.053(4) Uani 1 1 d . . . . .
H24A H -0.0725 0.4755 0.8756 0.063 Uiso 1 1 calc R U . . .
H24B H -0.1358 0.4454 0.8521 0.063 Uiso 1 1 calc R U . . .
C25 C -0.0411(8) 0.2327(8) 0.8333(4) 0.044(4) Uani 1 1 d . . . . .
O9 O -0.0149(6) 0.1966(5) 0.8074(3) 0.054(3) Uani 1 1 d . . . . .
N17 N -0.0701(7) 0.2939(7) 0.8267(3) 0.046(3) Uani 1 1 d . . . . .
N18 N -0.0464(7) 0.2218(6) 0.8732(3) 0.047(3) Uani 1 1 d . . . . .
C26 C -0.1054(8) 0.3205(7) 0.8621(4) 0.047(4) Uani 1 1 d . . . . .
H26 H -0.1604 0.3264 0.8611 0.056 Uiso 1 1 calc R U . . .
C27 C -0.0907(7) 0.2733(7) 0.8947(4) 0.043(3) Uani 1 1 d . . . . .
H27 H -0.1387 0.2560 0.9089 0.052 Uiso 1 1 calc R U . . .
N19 N -0.0494(7) 0.3068(6) 0.9208(3) 0.047(3) Uani 1 1 d . . . . .
N20 N -0.0706(7) 0.3797(6) 0.8738(4) 0.046(3) Uani 1 1 d . . . . .
C28 C -0.0374(8) 0.3744(7) 0.9111(4) 0.044(4) Uani 1 1 d . . . . .
O10 O -0.0212(5) 0.4149(4) 0.9326(2) 0.035(2) Uani 1 1 d . . . . .
C29 C -0.0390(7) 0.1577(7) 0.8904(4) 0.044(4) Uani 1 1 d . . . . .
H29A H -0.0870 0.1455 0.9062 0.053 Uiso 1 1 calc R U . . .
H29B H -0.0282 0.1262 0.8688 0.053 Uiso 1 1 calc R U . . .
C30 C -0.0460(8) 0.2854(8) 0.9612(4) 0.044(4) Uani 1 1 d . . . . .
H30A H -0.0388 0.3232 0.9779 0.053 Uiso 1 1 calc R U . . .
H30B H -0.0944 0.2650 0.9716 0.053 Uiso 1 1 calc R U . . .
C31 C 0.0750(6) 0.1121(7) 0.9090(3) 0.035(3) Uani 1 1 d . . . . .
O11 O 0.0942(5) 0.0836(5) 0.8776(3) 0.047(2) Uani 1 1 d . . . . .
N21 N 0.0205(6) 0.1554(5) 0.9156(3) 0.039(3) Uani 1 1 d . . . . .
N22 N 0.1099(6) 0.1040(6) 0.9420(3) 0.039(3) Uani 1 1 d . . . . .
C32 C 0.0059(7) 0.1735(7) 0.9557(4) 0.043(4) Uani 1 1 d . . . . .
H32 H -0.0433 0.1561 0.9683 0.052 Uiso 1 1 calc R U . . .
C33 C 0.0741(7) 0.1426(7) 0.9754(4) 0.041(3) Uani 1 1 d . . . . .
H33 H 0.0569 0.1157 0.9994 0.050 Uiso 1 1 calc R U . . .
N23 N 0.1168(5) 0.1981(6) 0.9848(3) 0.036(3) Uani 1 1 d D . . . .
N24 N 0.0135(6) 0.2405(6) 0.9642(3) 0.043(3) Uani 1 1 d . . . . .
C34 C 0.0774(8) 0.2536(7) 0.9815(4) 0.043(4) Uani 1 1 d . . . . .
O12 O 0.0970(5) 0.3072(5) 0.9911(3) 0.049(3) Uani 1 1 d . . . . .
C35 C 0.1641(9) 0.0561(8) 0.9477(5) 0.053(4) Uani 1 1 d . . . . .
H35A H 0.1639 0.0239 0.9264 0.064 Uiso 1 1 calc R U . . .
H35B H 0.1485 0.0339 0.9732 0.064 Uiso 1 1 calc R U . . .
C36 C 0.1726(5) 0.1936(8) 1.0124(4) 0.043(2) Uani 1 1 d D . . . .
H36A H 0.1786 0.2357 1.0250 0.052 Uiso 1 1 calc R U . . .
H36B H 0.1571 0.1613 1.0334 0.052 Uiso 1 1 calc R U . . .
C37 C 0.2965(7) 0.0582(6) 0.9204(4) 0.034(3) Uani 1 1 d . . . . .
O13 O 0.2903(5) 0.0279(5) 0.8909(3) 0.043(2) Uani 1 1 d . . . . .
N25 N 0.2408(6) 0.0795(6) 0.9477(3) 0.046(3) Uani 1 1 d . . . . .
N26 N 0.3636(6) 0.0803(6) 0.9316(3) 0.038(3) Uani 1 1 d . . . . .
C38 C 0.2646(6) 0.1055(8) 0.9818(5) 0.043(2) Uani 1 1 d . . . . .
H38 H 0.2508 0.0770 1.0055 0.052 Uiso 1 1 calc R U . . .
C39 C 0.3541(8) 0.1100(8) 0.9706(4) 0.044(4) Uani 1 1 d . . . . .
H39 H 0.3818 0.0864 0.9901 0.053 Uiso 1 1 calc R U . . .
N27 N 0.3678(5) 0.1773(6) 0.9705(4) 0.047(3) Uani 1 1 d . . . . .
N28 N 0.2397(5) 0.1751(6) 0.9903(4) 0.043(2) Uani 1 1 d D . . . .
C40 C 0.3075(7) 0.2137(8) 0.9842(4) 0.041(3) Uani 1 1 d . . . . .
O14 O 0.3081(5) 0.2693(5) 0.9921(3) 0.053(3) Uani 1 1 d . . . . .
C41 C 0.4359(8) 0.0564(7) 0.9133(4) 0.045(3) Uani 1 1 d . . . . .
H41A H 0.4632 0.0367 0.9340 0.054 Uiso 1 1 calc R U . . .
H41B H 0.4276 0.0226 0.8940 0.054 Uiso 1 1 calc R U . . .
C42 C 0.4446(8) 0.2003(8) 0.9704(4) 0.054(4) Uani 1 1 d . . . . .
H42A H 0.4427 0.2435 0.9825 0.065 Uiso 1 1 calc R U . . .
H42B H 0.4705 0.1713 0.9876 0.065 Uiso 1 1 calc R U . . .
C43 C 0.4992(7) 0.1098(7) 0.8524(3) 0.054(4) Uani 1 1 d . . . . .
O15 O 0.4726(6) 0.0760(5) 0.8288(3) 0.048(2) Uani 1 1 d . . . . .
N29 N 0.4806(6) 0.1063(6) 0.8936(3) 0.039(3) Uani 1 1 d . . . . .
N30 N 0.5530(6) 0.1555(6) 0.8439(3) 0.037(3) Uani 1 1 d . . . . .
C44 C 0.5272(7) 0.1475(7) 0.9138(4) 0.041(3) Uani 1 1 d . . . . .
H44 H 0.5544 0.1228 0.9331 0.049 Uiso 1 1 calc R U . . .
C45 C 0.5805(6) 0.1784(6) 0.8819(3) 0.029(3) Uani 1 1 d . . . . .
H45 H 0.6333 0.1643 0.8835 0.035 Uiso 1 1 calc R U . . .
N31 N 0.5727(7) 0.2467(6) 0.8870(3) 0.043(3) Uani 1 1 d . . . . .
N32 N 0.4887(6) 0.2044(6) 0.9325(3) 0.039(3) Uani 1 1 d . . . . .
C46 C 0.5184(7) 0.2608(7) 0.9165(4) 0.037(3) Uani 1 1 d . . . . .
O16 O 0.5009(5) 0.3156(5) 0.9290(3) 0.048(2) Uani 1 1 d . . . . .
C47 C 0.5959(8) 0.1622(8) 0.8044(4) 0.045(4) Uani 1 1 d . . . . .
H47A H 0.6499 0.1557 0.8066 0.053 Uiso 1 1 calc R U . . .
H47B H 0.5800 0.1283 0.7870 0.053 Uiso 1 1 calc R U . . .
C48 C 0.6227(8) 0.2960(7) 0.8678(4) 0.040(3) Uani 1 1 d . . . . .
H48A H 0.6750 0.2800 0.8658 0.048 Uiso 1 1 calc R U . . .
H48B H 0.6193 0.3347 0.8847 0.048 Uiso 1 1 calc R U . . .
C49 C 0.1838(9) 0.5563(7) 0.5766(4) 0.047(4) Uani 1 1 d . . . . .
O17 O 0.1890(6) 0.5249(5) 0.6074(3) 0.054(3) Uani 1 1 d . . . . .
N33 N 0.1186(5) 0.5806(5) 0.5663(3) 0.036(2) Uani 1 1 d D . . . .
N34 N 0.2406(6) 0.5717(6) 0.5475(3) 0.0418(12) Uani 1 1 d . . . . .
C50 C 0.1297(8) 0.6098(7) 0.5257(4) 0.042(3) Uani 1 1 d . . . . .
H50 H 0.0983 0.5882 0.5073 0.050 Uiso 1 1 calc R U . . .
C51 C 0.2156(7) 0.5999(7) 0.5127(4) 0.044(4) Uani 1 1 d . . . . .
H51 H 0.2260 0.5720 0.4888 0.052 Uiso 1 1 calc R U . . .
N35 N 0.2401(6) 0.6661(6) 0.5049(3) 0.0418(12) Uani 1 1 d D . . . .
N36 N 0.1207(6) 0.6806(5) 0.5250(3) 0.037(3) Uani 1 1 d D . . . .
C52 C 0.1826(8) 0.7094(8) 0.5090(4) 0.043(3) Uani 1 1 d . . . . .
O18 O 0.1897(5) 0.7684(5) 0.5007(3) 0.050(3) Uani 1 1 d . . . . .
C53 C 0.3146(8) 0.5464(7) 0.5480(4) 0.0418(12) Uani 1 1 d . . . . .
H53A H 0.3298 0.5235 0.5229 0.050 Uiso 1 1 calc R U . . .
H53B H 0.3139 0.5147 0.5700 0.050 Uiso 1 1 calc R U . . .
C54 C 0.3050(7) 0.6869(8) 0.4820(4) 0.0418(12) Uani 1 1 d D . . . .
H54A H 0.2975 0.7311 0.4723 0.050 Uiso 1 1 calc R U . . .
H54B H 0.3156 0.6586 0.4587 0.050 Uiso 1 1 calc R U . . .
C55 C 0.4035(7) 0.5993(6) 0.5868(3) 0.034(3) Uani 1 1 d . . . . .
O19 O 0.3856(6) 0.5695(5) 0.6180(3) 0.048(2) Uani 1 1 d . . . . .
N37 N 0.3694(6) 0.5953(6) 0.5529(3) 0.0418(12) Uani 1 1 d . . . . .
N38 N 0.4634(6) 0.6410(6) 0.5794(3) 0.039(3) Uani 1 1 d . . . . .
C56 C 0.4118(7) 0.6288(8) 0.5201(4) 0.043(4) Uani 1 1 d . . . . .
H56 H 0.4292 0.5988 0.4980 0.052 Uiso 1 1 calc R U . . .
C57 C 0.4795(8) 0.6591(7) 0.5382(4) 0.043(4) Uani 1 1 d . . . . .
H57 H 0.5288 0.6419 0.5258 0.051 Uiso 1 1 calc R U . . .
N39 N 0.4717(7) 0.7273(6) 0.5304(3) 0.048(3) Uani 1 1 d . . . . .
N40 N 0.3719(6) 0.6860(6) 0.5054(3) 0.0418(12) Uani 1 1 d D . . . .
C58 C 0.4117(8) 0.7410(9) 0.5102(4) 0.044(4) Uani 1 1 d . . . . .
O20 O 0.3966(6) 0.7950(6) 0.4970(4) 0.062(3) Uani 1 1 d . . . . .
C59 C 0.5202(9) 0.6429(8) 0.6081(4) 0.052(4) Uani 1 1 d . . . . .
H59A H 0.5055 0.6121 0.6301 0.062 Uiso 1 1 calc R U . . .
H59B H 0.5697 0.6295 0.5946 0.062 Uiso 1 1 calc R U . . .
C60 C 0.5305(8) 0.7744(8) 0.5349(4) 0.047(4) Uani 1 1 d . . . . .
H60A H 0.5238 0.8121 0.5176 0.057 Uiso 1 1 calc R U . . .
H60B H 0.5799 0.7550 0.5257 0.057 Uiso 1 1 calc R U . . .
C61 C 0.5122(8) 0.7154(8) 0.6647(4) 0.046(4) Uani 1 1 d . . . . .
O21 O 0.4824(6) 0.6775(5) 0.6894(3) 0.057(3) Uani 1 1 d . . . . .
N41 N 0.5260(6) 0.7051(6) 0.6237(3) 0.042(3) Uani 1 1 d . . . . .
N42 N 0.5349(8) 0.7750(6) 0.6718(3) 0.056(4) Uani 1 1 d . . . . .
C62 C 0.5676(9) 0.7584(7) 0.6037(4) 0.0503(14) Uani 1 1 d . . . . .
H62 H 0.6180 0.7437 0.5912 0.060 Uiso 1 1 calc R U . . .
C63 C 0.5760(9) 0.8057(7) 0.6371(4) 0.0503(14) Uani 1 1 d . . . . .
H63 H 0.6300 0.8123 0.6407 0.060 Uiso 1 1 calc R U . . .
N43 N 0.5416(7) 0.8663(6) 0.6221(3) 0.0503(14) Uani 1 1 d . . . . .
N44 N 0.5308(7) 0.7962(6) 0.5756(3) 0.0503(14) Uani 1 1 d . . . . .
C64 C 0.5230(9) 0.8556(8) 0.5872(4) 0.0503(14) Uani 1 1 d . . . . .
O22 O 0.4910(6) 0.9008(5) 0.5678(3) 0.0503(14) Uani 1 1 d . . . . .
C65 C 0.5478(12) 0.7945(8) 0.7118(5) 0.067(5) Uani 1 1 d . . . . .
H65A H 0.5374 0.7574 0.7302 0.080 Uiso 1 1 calc R U . . .
H65B H 0.6012 0.8063 0.7115 0.080 Uiso 1 1 calc R U . . .
C66 C 0.5473(10) 0.9273(7) 0.6394(5) 0.067(5) Uani 1 1 d . . . . .
H66A H 0.5341 0.9608 0.6205 0.080 Uiso 1 1 calc R U . . .
H66B H 0.6001 0.9345 0.6438 0.080 Uiso 1 1 calc R U . . .
C67 C 0.4572(9) 0.8452(7) 0.7607(4) 0.051(4) Uani 1 1 d . . . . .
O23 O 0.4394(7) 0.7960(5) 0.7806(3) 0.061(3) Uani 1 1 d . . . . .
N45 N 0.5021(8) 0.8476(6) 0.7264(4) 0.052(3) Uani 1 1 d . . . . .
N46 N 0.4378(7) 0.9078(6) 0.7722(3) 0.047(3) Uani 1 1 d . . . . .
C68 C 0.5216(8) 0.9131(8) 0.7142(4) 0.048(4) Uani 1 1 d . . . . .
H68 H 0.5762 0.9213 0.7152 0.057 Uiso 1 1 calc R U . . .
C69 C 0.4730(8) 0.9544(8) 0.7452(4) 0.049(4) Uani 1 1 d . . . . .
H69 H 0.5038 0.9856 0.7585 0.058 Uiso 1 1 calc R U . . .
N47 N 0.4207(6) 0.9874(6) 0.7208(3) 0.041(3) Uani 1 1 d . . . . .
N48 N 0.4993(7) 0.9353(6) 0.6771(3) 0.044(3) Uani 1 1 d . . . . .
C70 C 0.4422(9) 0.9809(7) 0.6817(4) 0.041(3) Uani 1 1 d . . . . .
O24 O 0.4174(6) 1.0073(5) 0.6542(3) 0.050(3) Uani 1 1 d . . . . .
C71 C 0.3968(9) 0.9231(8) 0.8116(4) 0.049(4) Uani 1 1 d . . . . .
H71A H 0.3949 0.8842 0.8287 0.059 Uiso 1 1 calc R U . . .
H71B H 0.4247 0.9567 0.8242 0.059 Uiso 1 1 calc R U . . .
C72 C 0.3794(7) 1.0443(6) 0.7364(4) 0.038(3) Uani 1 1 d . . . . .
H72A H 0.4110 1.0689 0.7529 0.046 Uiso 1 1 calc R U . . .
H72B H 0.3689 1.0723 0.7140 0.046 Uiso 1 1 calc R U . . .
C73 C 0.2621(8) 0.9115(8) 0.8284(4) 0.039(3) Uani 1 1 d . . . . .
O25 O 0.2644(7) 0.8552(6) 0.8424(3) 0.065(3) Uani 1 1 d . . . . .
N49 N 0.3234(7) 0.9447(6) 0.8094(3) 0.043(3) Uani 1 1 d . . . . .
N50 N 0.2006(6) 0.9496(5) 0.8291(3) 0.037(3) Uani 1 1 d . . . . .
C74 C 0.3066(8) 1.0104(6) 0.8025(3) 0.035(3) Uani 1 1 d . . . . .
H74 H 0.3360 1.0404 0.8174 0.042 Uiso 1 1 calc R U . . .
C75 C 0.2213(8) 1.0136(7) 0.8162(3) 0.038(3) Uani 1 1 d . . . . .
H75 H 0.2103 1.0447 0.8384 0.045 Uiso 1 1 calc R U . . .
N51 N 0.1891(6) 1.0360(5) 0.7810(3) 0.037(3) Uani 1 1 d . . . . .
N52 N 0.3103(6) 1.0279(5) 0.7597(3) 0.038(3) Uani 1 1 d . . . . .
C76 C 0.2412(8) 1.0444(7) 0.7488(4) 0.039(3) Uani 1 1 d . . . . .
O26 O 0.2311(6) 1.0658(5) 0.7162(3) 0.053(3) Uani 1 1 d . . . . .
C77 C 0.1308(8) 0.9314(7) 0.8510(4) 0.042(3) Uani 1 1 d . . . . .
H77A H 0.1160 0.9646 0.8711 0.051 Uiso 1 1 calc R U . . .
H77B H 0.1377 0.8904 0.8651 0.051 Uiso 1 1 calc R U . . .
C78 C 0.1145(6) 1.0609(6) 0.7820(3) 0.032(3) Uani 1 1 d . . . . .
H78A H 0.1129 1.0908 0.7593 0.038 Uiso 1 1 calc R U . . .
H78B H 0.1024 1.0859 0.8066 0.038 Uiso 1 1 calc R U . . .
C79 C 0.0411(8) 0.8658(7) 0.8201(3) 0.053(3) Uani 1 1 d . . . . .
O27 O 0.0665(6) 0.8136(6) 0.8311(3) 0.053(3) Uani 1 1 d . . . . .
N53 N 0.0698(7) 0.9235(6) 0.8263(3) 0.044(3) Uani 1 1 d . . . . .
N54 N -0.0222(7) 0.8706(6) 0.8018(3) 0.048(3) Uani 1 1 d . . . . .
C80 C -0.0409(7) 0.9393(7) 0.7988(4) 0.038(3) Uani 1 1 d . . . . .
H80 H -0.0903 0.9485 0.8147 0.045 Uiso 1 1 calc R U . . .
C81 C 0.0227(8) 0.9762(6) 0.8156(4) 0.036(3) Uani 1 1 d . . . . .
H81 H 0.0045 1.0046 0.8384 0.043 Uiso 1 1 calc R U . . .
N55 N -0.0397(7) 0.9639(6) 0.7596(3) 0.045(3) Uani 1 1 d . . . . .
N56 N 0.0567(7) 1.0116(6) 0.7806(3) 0.046(3) Uani 1 1 d . . . . .
C82 C 0.0126(8) 1.0081(6) 0.7508(4) 0.039(3) Uani 1 1 d . . . . .
O28 O 0.0252(5) 1.0411(5) 0.7193(3) 0.047(2) Uani 1 1 d . . . . .
C83 C -0.0716(9) 0.8180(7) 0.7990(4) 0.051(4) Uani 1 1 d . . . . .
H83A H -0.1216 0.8286 0.8131 0.061 Uiso 1 1 calc R U . . .
H83B H -0.0524 0.7798 0.8122 0.061 Uiso 1 1 calc R U . . .
C84 C -0.0995(9) 0.9541(7) 0.7369(4) 0.049(4) Uani 1 1 d . . . . .
H84A H -0.0996 0.9901 0.7176 0.059 Uiso 1 1 calc R U . . .
H84B H -0.1472 0.9562 0.7549 0.059 Uiso 1 1 calc R U . . .
C85 C -0.0662(7) 0.7393(8) 0.7455(4) 0.037(3) Uani 1 1 d . . . . .
O29 O -0.0342(6) 0.6970(5) 0.7609(3) 0.048(3) Uani 1 1 d . . . . .
N57 N -0.0793(7) 0.8024(5) 0.7579(3) 0.040(3) Uani 1 1 d . . . . .
N58 N -0.0969(6) 0.7346(6) 0.7092(3) 0.042(3) Uani 1 1 d . . . . .
C86 C -0.1381(7) 0.7905(7) 0.7000(4) 0.036(3) Uani 1 1 d . . . . .
H86 H -0.1922 0.7807 0.6984 0.044 Uiso 1 1 calc R U . . .
C87 C -0.1274(8) 0.8369(7) 0.7357(4) 0.039(3) Uani 1 1 d . . . . .
H87 H -0.1766 0.8455 0.7520 0.047 Uiso 1 1 calc R U . . .
N59 N -0.1047(6) 0.8274(6) 0.6663(3) 0.041(3) Uani 1 1 d . . . . .
N60 N -0.0986(6) 0.8945(5) 0.7153(3) 0.035(2) Uani 1 1 d . . . . .
C88 C -0.0916(6) 0.8916(7) 0.6747(3) 0.034(3) Uani 1 1 d . . . . .
O30 O -0.0732(6) 0.9329(5) 0.6525(3) 0.049(3) Uani 1 1 d . . . . .
C89 C -0.1070(8) 0.6735(7) 0.6921(4) 0.043(3) Uani 1 1 d . . . . .
H89A H -0.1609 0.6668 0.6900 0.051 Uiso 1 1 calc R U . . .
H89B H -0.0907 0.6393 0.7097 0.051 Uiso 1 1 calc R U . . .
C90 C -0.1202(7) 0.8108(8) 0.6269(4) 0.045(4) Uani 1 1 d . . . . .
H90A H -0.1739 0.7990 0.6282 0.054 Uiso 1 1 calc R U . . .
H90B H -0.1121 0.8496 0.6097 0.054 Uiso 1 1 calc R U . . .
C91 C -0.0128(7) 0.6193(7) 0.6453(4) 0.038(3) Uani 1 1 d . . . . .
O31 O 0.0146(5) 0.5865(5) 0.6689(3) 0.043(2) Uani 1 1 d . . . . .
N61 N -0.0641(5) 0.6687(6) 0.6529(3) 0.039(3) Uani 1 1 d D . . . .
N62 N 0.0033(6) 0.6136(5) 0.6039(3) 0.040(3) Uani 1 1 d D . . . .
C92 C -0.0887(5) 0.6945(5) 0.6170(3) 0.025(3) Uani 1 1 d D . . . .
H92 H -0.1426 0.6833 0.6160 0.030 Uiso 1 1 calc R U . . .
C93 C -0.0392(7) 0.6607(7) 0.5833(3) 0.040(3) Uani 1 1 d . . . . .
H93 H -0.0698 0.6396 0.5644 0.048 Uiso 1 1 calc R U . . .
N63 N 0.0055(5) 0.7129(5) 0.5647(3) 0.034(2) Uani 1 1 d D . . . .
N64 N -0.0774(6) 0.7608(5) 0.6091(3) 0.043(3) Uani 1 1 d D . . . .
C94 C -0.0172(7) 0.7708(7) 0.5809(4) 0.037(3) Uani 1 1 d . . . . .
O32 O 0.0100(5) 0.8228(5) 0.5710(3) 0.046(2) Uani 1 1 d . . . . .
C95 C 0.0459(7) 0.5617(6) 0.5851(4) 0.044(3) Uani 1 1 d D . . . .
H95A H 0.0174 0.5428 0.5649 0.053 Uiso 1 1 calc R U . . .
H95B H 0.0521 0.5279 0.6051 0.053 Uiso 1 1 calc R U . . .
C96 C 0.0465(7) 0.7092(8) 0.5252(3) 0.047(4) Uani 1 1 d D . . . .
H96A H 0.0519 0.7531 0.5136 0.057 Uiso 1 1 calc R U . . .
H96B H 0.0171 0.6833 0.5083 0.057 Uiso 1 1 calc R U . . .
Pt1 Pt 0.21218(3) 0.59810(3) 0.99778(2) 0.03852(14) Uani 1 1 d . . . . .
Cl1 Cl 0.2401(2) 0.66857(19) 1.04564(11) 0.0534(10) Uani 1 1 d . . . . .
N65 N 0.2141(6) 0.5154(6) 1.0291(3) 0.044(3) Uani 1 1 d . . . . .
C97 C 0.2250(7) 0.5102(9) 1.0688(4) 0.051(4) Uani 1 1 d . . . . .
H97 H 0.2317 0.5475 1.0839 0.061 Uiso 1 1 calc R U . . .
C98 C 0.2260(9) 0.4500(10) 1.0856(5) 0.062(5) Uani 1 1 d . . . . .
H98 H 0.2329 0.4462 1.1128 0.074 Uiso 1 1 calc R U . . .
C99 C 0.2177(12) 0.3977(10) 1.0655(6) 0.076(6) Uani 1 1 d . . . . .
H99 H 0.2186 0.3570 1.0785 0.091 Uiso 1 1 calc R U . . .
C100 C 0.2073(8) 0.4005(8) 1.0250(4) 0.047(4) Uani 1 1 d . . . . .
H100 H 0.2031 0.3628 1.0098 0.057 Uiso 1 1 calc R U . . .
C101 C 0.2037(7) 0.4618(8) 1.0085(4) 0.045(4) Uani 1 1 d . . . . .
C102 C 0.1907(7) 0.4742(7) 0.9669(4) 0.038(3) Uani 1 1 d . . . . .
C103 C 0.1801(7) 0.4300(8) 0.9375(4) 0.043(3) Uani 1 1 d . . . . .
H103 H 0.1780 0.3855 0.9440 0.051 Uiso 1 1 calc R U . . .
C104 C 0.1726(8) 0.4489(9) 0.8989(5) 0.061(5) Uani 1 1 d . . . . .
C105 C 0.1716(8) 0.5170(7) 0.8924(4) 0.043(3) Uani 1 1 d . . . . .
H105 H 0.1637 0.5326 0.8669 0.051 Uiso 1 1 calc R U . . .
C106 C 0.1816(7) 0.5610(7) 0.9214(4) 0.037(3) Uani 1 1 d . . . . .
N66 N 0.1906(6) 0.5354(7) 0.9585(4) 0.047(3) Uani 1 1 d . . . . .
C107 C 0.1852(8) 0.6299(8) 0.9186(5) 0.049(4) Uani 1 1 d . . . . .
C108 C 0.1724(9) 0.6675(9) 0.8861(5) 0.055(4) Uani 1 1 d . . . . .
H108 H 0.1588 0.6477 0.8629 0.066 Uiso 1 1 calc R U . . .
C109 C 0.1793(10) 0.7320(11) 0.8873(7) 0.077(6) Uani 1 1 d . . . . .
H109 H 0.1735 0.7555 0.8638 0.092 Uiso 1 1 calc R U . . .
C110 C 0.1936(10) 0.7656(11) 0.9188(6) 0.073(5) Uani 1 1 d . . . . .
H110 H 0.1962 0.8113 0.9190 0.088 Uiso 1 1 calc R U . . .
C111 C 0.2053(8) 0.7233(8) 0.9538(5) 0.055(4) Uani 1 1 d . . . . .
H111 H 0.2157 0.7430 0.9777 0.066 Uiso 1 1 calc R U . . .
N67 N 0.2016(6) 0.6593(6) 0.9526(3) 0.045(3) Uani 1 1 d . . . . .
C112 C 0.1653(8) 0.4021(10) 0.8677(4) 0.067(6) Uani 1 1 d . . . . .
C113 C 0.1871(8) 0.4199(10) 0.8271(5) 0.061(5) Uani 1 1 d . . . . .
H113 H 0.2034 0.4626 0.8206 0.073 Uiso 1 1 calc R U . . .
C114 C 0.1849(9) 0.3778(10) 0.7987(5) 0.069(5) Uani 1 1 d . . . . .
H114 H 0.1999 0.3904 0.7719 0.083 Uiso 1 1 calc R U . . .
C115 C 0.1611(7) 0.3155(10) 0.8071(4) 0.055(4) Uani 1 1 d . . . . .
C116 C 0.1366(8) 0.2992(9) 0.8459(5) 0.058(4) Uani 1 1 d . . . . .
H116 H 0.1172 0.2573 0.8519 0.070 Uiso 1 1 calc R U . . .
C117 C 0.1396(8) 0.3410(8) 0.8752(5) 0.057(4) Uani 1 1 d . . . . .
H117 H 0.1235 0.3280 0.9018 0.068 Uiso 1 1 calc R U . . .
C118 C 0.1586(11) 0.2659(12) 0.7728(7) 0.100(8) Uani 1 1 d . . . . .
H11C H 0.2035 0.2387 0.7710 0.150 Uiso 1 1 calc R U . . .
H11D H 0.1572 0.2891 0.7476 0.150 Uiso 1 1 calc R U . . .
H11E H 0.1137 0.2390 0.7783 0.150 Uiso 1 1 calc R U . . .
Pt2 Pt 0.39593(2) 0.60704(3) 0.95551(2) 0.03215(13) Uani 1 1 d . . . . .
Cl2 Cl 0.4255(2) 0.7026(2) 0.98302(12) 0.0589(11) Uani 1 1 d . . . . .
N68 N 0.4067(5) 0.5472(5) 1.0015(3) 0.032(2) Uani 1 1 d . . . . .
C119 C 0.4215(6) 0.5631(8) 1.0378(4) 0.044(4) Uani 1 1 d . . . . .
H119 H 0.4296 0.6069 1.0438 0.052 Uiso 1 1 calc R U . . .
C120 C 0.4249(7) 0.5163(9) 1.0664(4) 0.052(4) Uani 1 1 d . . . . .
H120 H 0.4335 0.5280 1.0925 0.062 Uiso 1 1 calc R U . . .
C121 C 0.4161(8) 0.4530(9) 1.0574(4) 0.048(4) Uani 1 1 d . . . . .
H121 H 0.4193 0.4214 1.0775 0.057 Uiso 1 1 calc R U . . .
C122 C 0.4027(7) 0.4333(8) 1.0206(4) 0.052(4) Uani 1 1 d . . . . .
H122 H 0.3962 0.3892 1.0147 0.062 Uiso 1 1 calc R U . . .
C123 C 0.3993(7) 0.4832(7) 0.9918(4) 0.035(3) Uani 1 1 d . . . . .
C124 C 0.3838(7) 0.4718(7) 0.9502(4) 0.036(3) Uani 1 1 d . . . . .
C125 C 0.3784(7) 0.4120(6) 0.9319(4) 0.037(3) Uani 1 1 d . . . . .
H125 H 0.3803 0.3726 0.9461 0.044 Uiso 1 1 calc R U . . .
C126 C 0.3700(6) 0.4138(7) 0.8911(4) 0.040(4) Uani 1 1 d . . . . .
C127 C 0.3639(7) 0.4721(7) 0.8720(4) 0.038(3) Uani 1 1 d . . . . .
H127 H 0.3547 0.4725 0.8451 0.045 Uiso 1 1 calc R U . . .
C128 C 0.3707(6) 0.5283(6) 0.8905(3) 0.029(3) Uani 1 1 d . . . . .
N69 N 0.3811(5) 0.5264(5) 0.9300(3) 0.031(2) Uani 1 1 d . . . . .
C129 C 0.3663(8) 0.5944(7) 0.8760(4) 0.041(3) Uani 1 1 d . . . . .
C130 C 0.3494(9) 0.6093(7) 0.8380(4) 0.043(3) Uani 1 1 d . . . . .
H130 H 0.3379 0.5763 0.8206 0.052 Uiso 1 1 calc R U . . .
C131 C 0.3497(11) 0.6703(9) 0.8266(5) 0.067(5) Uani 1 1 d . . . . .
H131 H 0.3426 0.6796 0.7999 0.080 Uiso 1 1 calc R U . . .
C132 C 0.3601(13) 0.7230(9) 0.8519(6) 0.083(6) Uani 1 1 d . . . . .
H132 H 0.3567 0.7665 0.8434 0.099 Uiso 1 1 calc R U . . .
C133 C 0.3754(9) 0.7067(7) 0.8899(4) 0.046(4) Uani 1 1 d . . . . .
H133 H 0.3839 0.7398 0.9079 0.055 Uiso 1 1 calc R U . . .
N70 N 0.3784(6) 0.6440(5) 0.9018(3) 0.036(3) Uani 1 1 d . . . . .
C134 C 0.3657(7) 0.3528(7) 0.8700(4) 0.039(3) Uani 1 1 d . . . . .
C135 C 0.3879(9) 0.3468(8) 0.8316(5) 0.057(4) Uani 1 1 d . . . . .
H135 H 0.4127 0.3829 0.8186 0.068 Uiso 1 1 calc R U . . .
C136 C 0.3791(10) 0.2934(9) 0.8081(5) 0.062(5) Uani 1 1 d . . . . .
H136 H 0.3943 0.2930 0.7803 0.075 Uiso 1 1 calc R U . . .
C137 C 0.3436(10) 0.2371(9) 0.8304(7) 0.072(6) Uani 1 1 d . . . . .
C138 C 0.3230(11) 0.2429(9) 0.8691(7) 0.073(5) Uani 1 1 d . . . . .
H138 H 0.3002 0.2071 0.8834 0.088 Uiso 1 1 calc R U . . .
C139 C 0.3334(10) 0.2994(8) 0.8896(5) 0.058(4) Uani 1 1 d . . . . .
H139 H 0.3180 0.3011 0.9173 0.070 Uiso 1 1 calc R U . . .
C140 C 0.3313(16) 0.1748(11) 0.8082(8) 0.128(11) Uani 1 1 d . . . . .
H14A H 0.3481 0.1380 0.8231 0.192 Uiso 1 1 calc R U . . .
H14B H 0.3601 0.1766 0.7818 0.192 Uiso 1 1 calc R U . . .
H14C H 0.2778 0.1700 0.8056 0.192 Uiso 1 1 calc R U . . .
Pt3 Pt 0.10417(2) 1.10290(2) 0.54602(2) 0.02874(12) Uani 1 1 d . . . . .
Cl3 Cl 0.0830(2) 1.1853(2) 0.50367(12) 0.0569(10) Uani 1 1 d . . . . .
N71 N 0.0987(5) 1.0262(6) 0.5094(3) 0.037(3) Uani 1 1 d . . . . .
C141 C 0.0876(7) 1.0292(9) 0.4712(3) 0.048(4) Uani 1 1 d . . . . .
H141 H 0.0815 1.0696 0.4587 0.058 Uiso 1 1 calc R U . . .
C142 C 0.0852(7) 0.9711(8) 0.4494(4) 0.049(4) Uani 1 1 d . . . . .
H142 H 0.0784 0.9718 0.4221 0.059 Uiso 1 1 calc R U . . .
C143 C 0.0929(7) 0.9153(9) 0.4688(4) 0.053(4) Uani 1 1 d . . . . .
H143 H 0.0900 0.8768 0.4542 0.063 Uiso 1 1 calc R U . . .
C144 C 0.1050(6) 0.9087(7) 0.5095(4) 0.044(4) Uani 1 1 d . . . . .
H144 H 0.1106 0.8686 0.5224 0.053 Uiso 1 1 calc R U . . .
C145 C 0.1075(6) 0.9688(7) 0.5281(4) 0.033(3) Uani 1 1 d . . . . .
C146 C 0.1165(7) 0.9711(7) 0.5718(4) 0.037(3) Uani 1 1 d . . . . .
C147 C 0.1220(7) 0.9222(7) 0.5992(4) 0.039(3) Uani 1 1 d . . . . .
H147 H 0.1185 0.8784 0.5918 0.047 Uiso 1 1 calc R U . . .
C148 C 0.1325(8) 0.9383(7) 0.6374(4) 0.045(4) Uani 1 1 d . . . . .
C149 C 0.1357(8) 1.0006(7) 0.6481(4) 0.043(3) Uani 1 1 d . . . . .
H149 H 0.1429 1.0112 0.6745 0.052 Uiso 1 1 calc R U . . .
C150 C 0.1283(7) 1.0500(6) 0.6202(3) 0.034(3) Uani 1 1 d . . . . .
N72 N 0.1206(5) 1.0322(5) 0.5824(3) 0.031(2) Uani 1 1 d . . . . .
C151 C 0.1240(7) 1.1160(7) 0.6276(3) 0.040(3) Uani 1 1 d . . . . .
C152 C 0.1286(11) 1.1478(9) 0.6625(4) 0.067(5) Uani 1 1 d . . . . .
H152 H 0.1342 1.1238 0.6859 0.080 Uiso 1 1 calc R U . . .
C153 C 0.1250(10) 1.2139(9) 0.6640(5) 0.063(5) Uani 1 1 d . . . . .
H153 H 0.1329 1.2352 0.6878 0.076 Uiso 1 1 calc R U . . .
C154 C 0.1110(9) 1.2472(8) 0.6334(5) 0.059(5) Uani 1 1 d . . . . .
H154 H 0.1041 1.2925 0.6354 0.071 Uiso 1 1 calc R U . . .
C155 C 0.1061(8) 1.2174(7) 0.5982(5) 0.050(4) Uani 1 1 d . . . . .
H155 H 0.0984 1.2431 0.5757 0.060 Uiso 1 1 calc R U . . .
N73 N 0.1115(5) 1.1555(5) 0.5940(3) 0.031(2) Uani 1 1 d . . . . .
C156 C 0.1348(7) 0.8862(7) 0.6681(3) 0.041(3) Uani 1 1 d . . . . .
C157 C 0.1752(10) 0.8967(8) 0.7002(4) 0.058(4) Uani 1 1 d . . . . .
H157 H 0.2001 0.9366 0.7025 0.069 Uiso 1 1 calc R U . . .
C158 C 0.1791(13) 0.8478(10) 0.7294(5) 0.083(6) Uani 1 1 d . . . . .
H158 H 0.2047 0.8564 0.7517 0.100 Uiso 1 1 calc R U . . .
C159 C 0.1451(10) 0.7856(8) 0.7262(5) 0.064(5) Uani 1 1 d . . . . .
C160 C 0.1093(9) 0.7787(8) 0.6925(5) 0.050(4) Uani 1 1 d . . . . .
H160 H 0.0864 0.7386 0.6883 0.059 Uiso 1 1 calc R U . . .
C161 C 0.1054(9) 0.8270(8) 0.6649(4) 0.052(4) Uani 1 1 d . . . . .
H161 H 0.0806 0.8183 0.6424 0.062 Uiso 1 1 calc R U . . .
C162 C 0.1519(11) 0.7330(9) 0.7546(5) 0.066(5) Uani 1 1 d . . . . .
H16A H 0.1031 0.7253 0.7702 0.098 Uiso 1 1 calc R U . . .
H16B H 0.1887 0.7448 0.7723 0.098 Uiso 1 1 calc R U . . .
H16C H 0.1685 0.6939 0.7402 0.098 Uiso 1 1 calc R U . . .
Pt4 Pt 0.28950(3) 1.09659(3) 0.48962(2) 0.04422(16) Uani 1 1 d . . . . .
Cl4 Cl 0.2747(2) 1.1833(2) 0.44858(13) 0.0651(11) Uani 1 1 d . . . . .
N74 N 0.2816(5) 1.0261(6) 0.4476(3) 0.042(3) Uani 1 1 d . . . . .
C163 C 0.2678(9) 1.0390(10) 0.4106(4) 0.062(5) Uani 1 1 d . . . . .
H163 H 0.2598 1.0819 0.4021 0.074 Uiso 1 1 calc R U . . .
C164 C 0.2657(10) 0.9864(12) 0.3843(5) 0.085(7) Uani 1 1 d . . . . .
H164 H 0.2591 0.9939 0.3573 0.102 Uiso 1 1 calc R U . . .
C165 C 0.2732(9) 0.9233(10) 0.3984(4) 0.060(5) Uani 1 1 d . . . . .
H165 H 0.2676 0.8876 0.3818 0.072 Uiso 1 1 calc R U . . .
C166 C 0.2891(8) 0.9136(8) 0.4379(4) 0.048(4) Uani 1 1 d . . . . .
H166 H 0.3003 0.8722 0.4477 0.057 Uiso 1 1 calc R U . . .
C167 C 0.2875(8) 0.9678(9) 0.4611(4) 0.054(4) Uani 1 1 d . . . . .
C168 C 0.3001(7) 0.9643(7) 0.5044(4) 0.040(3) Uani 1 1 d . . . . .
C169 C 0.3046(6) 0.9098(7) 0.5269(4) 0.035(3) Uani 1 1 d . . . . .
H169 H 0.3029 0.8685 0.5153 0.042 Uiso 1 1 calc R U . . .
C170 C 0.3114(7) 0.9156(7) 0.5660(4) 0.037(3) Uani 1 1 d . . . . .
C171 C 0.3169(7) 0.9725(7) 0.5847(5) 0.043(3) Uani 1 1 d . . . . .
H171 H 0.3240 0.9757 0.6118 0.051 Uiso 1 1 calc R U . . .
C172 C 0.3103(7) 1.0297(7) 0.5581(5) 0.049(4) Uani 1 1 d . . . . .
N75 N 0.3020(6) 1.0228(6) 0.5211(3) 0.045(3) Uani 1 1 d . . . . .
C173 C 0.3108(7) 1.0974(9) 0.5703(5) 0.057(4) Uani 1 1 d . . . . .
C174 C 0.3169(10) 1.1186(9) 0.6090(5) 0.066(5) Uani 1 1 d . . . . .
H174 H 0.3247 1.0890 0.6296 0.079 Uiso 1 1 calc R U . . .
C175 C 0.3110(11) 1.1846(11) 0.6160(6) 0.078(6) Uani 1 1 d . . . . .
H175 H 0.3151 1.2002 0.6418 0.094 Uiso 1 1 calc R U . . .
C176 C 0.2992(12) 1.2285(13) 0.5856(7) 0.097(8) Uani 1 1 d . . . . .
H176 H 0.2936 1.2733 0.5903 0.116 Uiso 1 1 calc R U . . .
C177 C 0.2962(9) 1.2031(9) 0.5489(6) 0.069(5) Uani 1 1 d . . . . .
H177 H 0.2905 1.2323 0.5278 0.083 Uiso 1 1 calc R U . . .
N76 N 0.3005(6) 1.1419(7) 0.5405(4) 0.050(3) Uani 1 1 d . . . . .
C178 C 0.3093(9) 0.8551(7) 0.5941(4) 0.045(4) Uani 1 1 d . . . . .
C179 C 0.3413(8) 0.8548(8) 0.6289(4) 0.053(4) Uani 1 1 d . . . . .
H179 H 0.3678 0.8918 0.6358 0.063 Uiso 1 1 calc R U . . .
C180 C 0.3359(10) 0.8028(8) 0.6535(4) 0.059(4) Uani 1 1 d . . . . .
H180 H 0.3563 0.8056 0.6779 0.071 Uiso 1 1 calc R U . . .
C181 C 0.3014(9) 0.7451(9) 0.6446(4) 0.057(4) Uani 1 1 d . . . . .
C182 C 0.2682(12) 0.7438(9) 0.6084(6) 0.080(6) Uani 1 1 d . . . . .
H182 H 0.2420 0.7066 0.6016 0.095 Uiso 1 1 calc R U . . .
C183 C 0.2746(10) 0.7991(9) 0.5823(5) 0.069(5) Uani 1 1 d . . . . .
H183 H 0.2556 0.7977 0.5574 0.083 Uiso 1 1 calc R U . . .
C184 C 0.2936(14) 0.6875(10) 0.6720(6) 0.089(7) Uani 1 1 d . . . . .
H18C H 0.2533 0.6597 0.6649 0.134 Uiso 1 1 calc R U . . .
H18D H 0.2814 0.7019 0.6994 0.134 Uiso 1 1 calc R U . . .
H18E H 0.3409 0.6635 0.6694 0.134 Uiso 1 1 calc R U . . .
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Cl Cl 0.1484 0.1585 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Pt Pt -1.7033 8.3905 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
O1 C1 N2 126.1(13) . . ?
O1 C1 N1 126.6(14) . . ?
N2 C1 N1 107.3(12) . . ?
C1 N1 C47 120.8(12) . . ?
C1 N1 C2 111.4(12) . . ?
C47 N1 C2 125.7(12) . . ?
C1 N2 C3 112.5(11) . . ?
C1 N2 C5 120.5(12) . . ?
C3 N2 C5 123.0(13) . . ?
N4 C2 N1 116.1(12) . . ?
N4 C2 C3 104.4(12) . . ?
N1 C2 C3 104.7(12) . . ?
N4 C2 H2 110.5 . . ?
N1 C2 H2 110.4 . . ?
C3 C2 H2 110.4 . . ?
N2 C3 N3 115.6(13) . . ?
N2 C3 C2 103.6(12) . . ?
N3 C3 C2 102.1(11) . . ?
N2 C3 H3 111.6 . . ?
N3 C3 H3 111.6 . . ?
C2 C3 H3 111.6 . . ?
C4 N3 C3 112.1(14) . . ?
C4 N3 C6 123.9(13) . . ?
C3 N3 C6 120.9(12) . . ?
C4 N4 C2 110.8(12) . . ?
C4 N4 C48 121.7(12) . . ?
C2 N4 C48 124.6(12) . . ?
O2 C4 N3 125.3(18) . . ?
O2 C4 N4 124.6(16) . . ?
N3 C4 N4 109.7(13) . . ?
N5 C5 N2 114.5(12) . . ?
N5 C5 H5A 108.7 . . ?
N2 C5 H5A 108.7 . . ?
N5 C5 H5B 108.6 . . ?
N2 C5 H5B 108.6 . . ?
H5A C5 H5B 107.6 . . ?
N8 C6 N3 112.5(12) . . ?
N8 C6 H6A 109.1 . . ?
N3 C6 H6A 109.1 . . ?
N8 C6 H6B 109.1 . . ?
N3 C6 H6B 109.1 . . ?
H6A C6 H6B 107.8 . . ?
O3 C7 N6 124.2(15) . . ?
O3 C7 N5 127.3(15) . . ?
N6 C7 N5 108.4(12) . . ?
C7 N5 C5 119.9(12) . . ?
C7 N5 C8 110.2(12) . . ?
C5 N5 C8 124.9(14) . . ?
C7 N6 C11 125.1(12) . . ?
C7 N6 C9 112.6(11) . . ?
C11 N6 C9 121.5(12) . . ?
N5 C8 N8 113.6(12) . . ?
N5 C8 C9 106.9(12) . . ?
N8 C8 C9 104.2(11) . . ?
N5 C8 H8 110.6 . . ?
N8 C8 H8 110.6 . . ?
C9 C8 H8 110.6 . . ?
N7 C9 N6 114.6(12) . . ?
N7 C9 C8 103.3(10) . . ?
N6 C9 C8 101.2(11) . . ?
N7 C9 H9 112.3 . . ?
N6 C9 H9 112.3 . . ?
C8 C9 H9 112.3 . . ?
C10 N7 C9 113.0(11) . . ?
C10 N7 C12 119.0(11) . . ?
C9 N7 C12 120.7(10) . . ?
C10 N8 C6 123.7(11) . . ?
C10 N8 C8 110.2(11) . . ?
C6 N8 C8 123.5(11) . . ?
O4 C10 N7 128.8(14) . . ?
O4 C10 N8 123.0(13) . . ?
N7 C10 N8 108.2(11) . . ?
N9 C11 N6 113.7(10) . . ?
N9 C11 H11A 108.8 . . ?
N6 C11 H11A 108.8 . . ?
N9 C11 H11B 108.8 . . ?
N6 C11 H11B 108.8 . . ?
H11A C11 H11B 107.7 . . ?
N12 C12 N7 111.7(11) . . ?
N12 C12 H12A 109.3 . . ?
N7 C12 H12A 109.3 . . ?
N12 C12 H12B 109.3 . . ?
N7 C12 H12B 109.3 . . ?
H12A C12 H12B 107.9 . . ?
O5 C13 N10 126.6(13) . . ?
O5 C13 N9 120.8(13) . . ?
N10 C13 N9 112.3(11) . . ?
C13 N9 C11 124.2(11) . . ?
C13 N9 C14 108.8(11) . . ?
C11 N9 C14 121.7(11) . . ?
C13 N10 C17 122.4(11) . . ?
C13 N10 C15 111.3(11) . . ?
C17 N10 C15 124.3(13) . . ?
N12 C14 N9 115.1(11) . . ?
N12 C14 C15 102.0(10) . . ?
N9 C14 C15 102.4(9) . . ?
N12 C14 H14 112.1 . . ?
N9 C14 H14 112.1 . . ?
C15 C14 H14 112.1 . . ?
N11 C15 N10 116.9(11) . . ?
N11 C15 C14 104.2(11) . . ?
N10 C15 C14 104.7(11) . . ?
N11 C15 H15 110.2 . . ?
N10 C15 H15 110.2 . . ?
C14 C15 H15 110.2 . . ?
C16 N11 C15 112.1(10) . . ?
C16 N11 C18 122.4(10) . . ?
C15 N11 C18 123.7(12) . . ?
C16 N12 C12 125.1(10) . . ?
C16 N12 C14 112.7(11) . . ?
C12 N12 C14 120.0(10) . . ?
O6 C16 N12 125.4(13) . . ?
O6 C16 N11 125.7(13) . . ?
N12 C16 N11 108.9(10) . . ?
N10 C17 N13 114.4(12) . . ?
N10 C17 H17A 108.7 . . ?
N13 C17 H17A 108.7 . . ?
N10 C17 H17B 108.7 . . ?
N13 C17 H17B 108.7 . . ?
H17A C17 H17B 107.6 . . ?
N11 C18 N16 113.2(11) . . ?
N11 C18 H18A 108.9 . . ?
N16 C18 H18A 108.9 . . ?
N11 C18 H18B 108.9 . . ?
N16 C18 H18B 108.9 . . ?
H18A C18 H18B 107.7 . . ?
O7 C19 N14 128.3(14) . . ?
O7 C19 N13 124.8(14) . . ?
N14 C19 N13 106.9(11) . . ?
C19 N13 C20 112.6(11) . . ?
C19 N13 C17 123.1(12) . . ?
C20 N13 C17 123.4(12) . . ?
C19 N14 C21 112.9(11) . . ?
C19 N14 C23 120.3(12) . . ?
C21 N14 C23 124.3(12) . . ?
N13 C20 N16 114.5(12) . . ?
N13 C20 C21 103.1(11) . . ?
N16 C20 C21 103.0(10) . . ?
N13 C20 H20 111.8 . . ?
N16 C20 H20 111.8 . . ?
C21 C20 H20 111.9 . . ?
N14 C21 N15 114.7(12) . . ?
N14 C21 C20 103.9(11) . . ?
N15 C21 C20 102.9(9) . . ?
N14 C21 H21 111.6 . . ?
N15 C21 H21 111.6 . . ?
C20 C21 H21 111.5 . . ?
C22 N15 C24 124.8(11) . . ?
C22 N15 C21 112.8(10) . . ?
C24 N15 C21 119.7(11) . . ?
C22 N16 C18 121.8(10) . . ?
C22 N16 C20 111.7(10) . . ?
C18 N16 C20 122.9(12) . . ?
O8 C22 N15 126.8(12) . . ?
O8 C22 N16 124.2(12) . . ?
N15 C22 N16 109.0(10) . . ?
N14 C23 N17 114.4(12) . . ?
N14 C23 H23A 108.7 . . ?
N17 C23 H23A 108.6 . . ?
N14 C23 H23B 108.7 . . ?
N17 C23 H23B 108.6 . . ?
H23A C23 H23B 107.6 . . ?
N20 C24 N15 113.0(13) . . ?
N20 C24 H24A 108.9 . . ?
N15 C24 H24A 108.9 . . ?
N20 C24 H24B 109.0 . . ?
N15 C24 H24B 109.0 . . ?
H24A C24 H24B 107.8 . . ?
O9 C25 N18 126.7(16) . . ?
O9 C25 N17 124.8(13) . . ?
N18 C25 N17 108.5(12) . . ?
C25 N17 C26 111.4(12) . . ?
C25 N17 C23 120.9(12) . . ?
C26 N17 C23 123.3(14) . . ?
C25 N18 C29 122.7(12) . . ?
C25 N18 C27 110.3(13) . . ?
C29 N18 C27 122.1(10) . . ?
N17 C26 N20 114.1(11) . . ?
N17 C26 C27 105.5(13) . . ?
N20 C26 C27 102.9(11) . . ?
N17 C26 H26 111.3 . . ?
N20 C26 H26 111.4 . . ?
C27 C26 H26 111.3 . . ?
N19 C27 N18 112.5(12) . . ?
N19 C27 C26 106.9(11) . . ?
N18 C27 C26 103.6(10) . . ?
N19 C27 H27 111.2 . . ?
N18 C27 H27 111.2 . . ?
C26 C27 H27 111.2 . . ?
C27 N19 C30 122.1(11) . . ?
C27 N19 C28 114.6(12) . . ?
C30 N19 C28 118.8(11) . . ?
C24 N20 C26 123.7(12) . . ?
C24 N20 C28 120.5(11) . . ?
C26 N20 C28 114.2(12) . . ?
O10 C28 N19 126.7(13) . . ?
O10 C28 N20 130.0(14) . . ?
N19 C28 N20 101.3(11) . . ?
N21 C29 N18 111.8(11) . . ?
N21 C29 H29A 109.2 . . ?
N18 C29 H29A 109.3 . . ?
N21 C29 H29B 109.3 . . ?
N18 C29 H29B 109.3 . . ?
H29A C29 H29B 107.9 . . ?
N24 C30 N19 112.3(12) . . ?
N24 C30 H30A 109.1 . . ?
N19 C30 H30A 109.1 . . ?
N24 C30 H30B 109.2 . . ?
N19 C30 H30B 109.2 . . ?
H30A C30 H30B 107.9 . . ?
O11 C31 N21 126.8(12) . . ?
O11 C31 N22 123.2(13) . . ?
N21 C31 N22 110.0(11) . . ?
C31 N21 C32 113.3(12) . . ?
C31 N21 C29 119.9(11) . . ?
C32 N21 C29 120.1(11) . . ?
C31 N22 C35 125.8(12) . . ?
C31 N22 C33 111.8(11) . . ?
C35 N22 C33 121.3(12) . . ?
N21 C32 N24 116.8(11) . . ?
N21 C32 C33 103.6(11) . . ?
N24 C32 C33 101.9(10) . . ?
N21 C32 H32 111.3 . . ?
N24 C32 H32 111.3 . . ?
C33 C32 H32 111.2 . . ?
N23 C33 N22 114.7(10) . . ?
N23 C33 C32 103.2(11) . . ?
N22 C33 C32 100.3(10) . . ?
N23 C33 H33 112.5 . . ?
N22 C33 H33 112.5 . . ?
C32 C33 H33 112.5 . . ?
C34 N23 C33 111.4(11) . . ?
C34 N23 C36 120.5(11) . . ?
C33 N23 C36 121.4(12) . . ?
C34 N24 C30 124.5(12) . . ?
C34 N24 C32 112.7(12) . . ?
C30 N24 C32 122.0(12) . . ?
O12 C34 N23 125.4(13) . . ?
O12 C34 N24 125.2(15) . . ?
N23 C34 N24 109.3(11) . . ?
N22 C35 N25 115.4(12) . . ?
N22 C35 H35A 108.4 . . ?
N25 C35 H35A 108.5 . . ?
N22 C35 H35B 108.4 . . ?
N25 C35 H35B 108.4 . . ?
H35A C35 H35B 107.5 . . ?
N28 C36 N23 106.7(11) . . ?
N28 C36 H36A 111.0 . . ?
N23 C36 H36A 110.5 . . ?
N28 C36 H36B 109.2 . . ?
N23 C36 H36B 110.6 . . ?
H36A C36 H36B 108.8 . . ?
O13 C37 N25 127.5(12) . . ?
O13 C37 N26 125.2(12) . . ?
N25 C37 N26 107.2(11) . . ?
C37 N25 C38 115.1(11) . . ?
C37 N25 C35 120.4(11) . . ?
C38 N25 C35 121.1(10) . . ?
C37 N26 C41 121.8(11) . . ?
C37 N26 C39 112.6(10) . . ?
C41 N26 C39 122.3(11) . . ?
N25 C38 N28 114.7(13) . . ?
N25 C38 C39 103.0(10) . . ?
N28 C38 C39 104.5(10) . . ?
N25 C38 H38 111.6 . . ?
N28 C38 H38 111.0 . . ?
C39 C38 H38 111.5 . . ?
N27 C39 N26 115.0(12) . . ?
N27 C39 C38 103.0(11) . . ?
N26 C39 C38 101.1(10) . . ?
N27 C39 H39 112.2 . . ?
N26 C39 H39 112.2 . . ?
C38 C39 H39 112.4 . . ?
C40 N27 C39 114.9(11) . . ?
C40 N27 C42 122.0(12) . . ?
C39 N27 C42 119.2(12) . . ?
C36 N28 C40 125.2(12) . . ?
C36 N28 C38 125.3(11) . . ?
C40 N28 C38 105.9(9) . . ?
O14 C40 N27 126.5(12) . . ?
O14 C40 N28 122.4(12) . . ?
N27 C40 N28 111.0(12) . . ?
N29 C41 N26 111.8(12) . . ?
N29 C41 H41A 109.3 . . ?
N26 C41 H41A 109.3 . . ?
N29 C41 H41B 109.2 . . ?
N26 C41 H41B 109.2 . . ?
H41A C41 H41B 107.9 . . ?
N32 C42 N27 116.0(12) . . ?
N32 C42 H42A 108.3 . . ?
N27 C42 H42A 108.3 . . ?
N32 C42 H42B 108.3 . . ?
N27 C42 H42B 108.2 . . ?
H42A C42 H42B 107.4 . . ?
O15 C43 N30 126.5(11) . . ?
O15 C43 N29 124.9(13) . . ?
N30 C43 N29 108.6(11) . . ?
C43 N29 C41 123.6(11) . . ?
C43 N29 C44 111.9(11) . . ?
C41 N29 C44 122.5(11) . . ?
C43 N30 C47 122.3(11) . . ?
C43 N30 C45 109.9(9) . . ?
C47 N30 C45 124.1(10) . . ?
N29 C44 N32 114.8(11) . . ?
N29 C44 C45 105.4(10) . . ?
N32 C44 C45 101.2(11) . . ?
N29 C44 H44 111.6 . . ?
N32 C44 H44 111.6 . . ?
C45 C44 H44 111.7 . . ?
N31 C45 C44 106.7(10) . . ?
N31 C45 N30 112.6(10) . . ?
C44 C45 N30 103.6(9) . . ?
N31 C45 H45 111.2 . . ?
C44 C45 H45 111.2 . . ?
N30 C45 H45 111.2 . . ?
C46 N31 C45 111.3(11) . . ?
C46 N31 C48 121.7(13) . . ?
C45 N31 C48 126.4(11) . . ?
C46 N32 C42 123.3(12) . . ?
C46 N32 C44 112.1(10) . . ?
C42 N32 C44 121.6(12) . . ?
O16 C46 N31 126.1(14) . . ?
O16 C46 N32 125.3(12) . . ?
N31 C46 N32 108.5(12) . . ?
N1 C47 N30 112.3(11) . . ?
N1 C47 H47A 109.1 . . ?
N30 C47 H47A 109.1 . . ?
N1 C47 H47B 109.2 . . ?
N30 C47 H47B 109.2 . . ?
H47A C47 H47B 107.9 . . ?
N31 C48 N4 113.7(11) . . ?
N31 C48 H48A 108.9 . . ?
N4 C48 H48A 108.8 . . ?
N31 C48 H48B 108.8 . . ?
N4 C48 H48B 108.8 . . ?
H48A C48 H48B 107.7 . . ?
O17 C49 N33 124.4(13) . . ?
O17 C49 N34 126.9(15) . . ?
N33 C49 N34 108.7(13) . . ?
C49 N33 C95 123.6(12) . . ?
C49 N33 C50 111.3(10) . . ?
C95 N33 C50 121.8(11) . . ?
C49 N34 C53 121.2(12) . . ?
C49 N34 C51 114.0(12) . . ?
C53 N34 C51 122.9(10) . . ?
N36 C50 N33 113.9(10) . . ?
N36 C50 C51 103.5(11) . . ?
N33 C50 C51 102.8(11) . . ?
N36 C50 H50 112.0 . . ?
N33 C50 H50 112.0 . . ?
C51 C50 H50 112.0 . . ?
N34 C51 N35 114.2(11) . . ?
N34 C51 C50 102.6(10) . . ?
N35 C51 C50 101.0(11) . . ?
N34 C51 H51 112.7 . . ?
N35 C51 H51 112.6 . . ?
C50 C51 H51 112.7 . . ?
C52 N35 C54 115.4(12) . . ?
C52 N35 C51 113.3(11) . . ?
C54 N35 C51 127.2(12) . . ?
C52 N36 C96 122.8(12) . . ?
C52 N36 C50 111.5(11) . . ?
C96 N36 C50 120.3(11) . . ?
O18 C52 N36 126.0(13) . . ?
O18 C52 N35 124.4(13) . . ?
N36 C52 N35 109.4(13) . . ?
N34 C53 N37 113.0(13) . . ?
N34 C53 H53A 108.9 . . ?
N37 C53 H53A 108.9 . . ?
N34 C53 H53B 109.0 . . ?
N37 C53 H53B 109.0 . . ?
H53A C53 H53B 107.8 . . ?
N35 C54 N40 111.6(10) . . ?
N35 C54 H54A 108.0 . . ?
N40 C54 H54A 108.6 . . ?
N35 C54 H54B 110.2 . . ?
N40 C54 H54B 110.4 . . ?
H54A C54 H54B 107.9 . . ?
O19 C55 N37 126.4(12) . . ?
O19 C55 N38 125.5(12) . . ?
N37 C55 N38 108.1(11) . . ?
C55 N37 C53 121.8(11) . . ?
C55 N37 C56 111.5(11) . . ?
C53 N37 C56 123.5(11) . . ?
C55 N38 C57 113.1(11) . . ?
C55 N38 C59 118.8(11) . . ?
C57 N38 C59 123.7(11) . . ?
N37 C56 N40 113.7(10) . . ?
N37 C56 C57 104.6(10) . . ?
N40 C56 C57 103.6(12) . . ?
N37 C56 H56 111.5 . . ?
N40 C56 H56 111.5 . . ?
C57 C56 H56 111.5 . . ?
N38 C57 N39 114.3(11) . . ?
N38 C57 C56 101.9(10) . . ?
N39 C57 C56 103.2(12) . . ?
N38 C57 H57 112.2 . . ?
N39 C57 H57 112.2 . . ?
C56 C57 H57 112.1 . . ?
C58 N39 C57 112.7(13) . . ?
C58 N39 C60 122.5(14) . . ?
C57 N39 C60 123.2(13) . . ?
C58 N40 C56 110.0(11) . . ?
C58 N40 C54 121.0(13) . . ?
C56 N40 C54 128.2(12) . . ?
O20 C58 N40 124.6(14) . . ?
O20 C58 N39 125.3(15) . . ?
N40 C58 N39 110.1(15) . . ?
N41 C59 N38 111.3(13) . . ?
N41 C59 H59A 109.4 . . ?
N38 C59 H59A 109.4 . . ?
N41 C59 H59B 109.4 . . ?
N38 C59 H59B 109.4 . . ?
H59A C59 H59B 108.0 . . ?
N39 C60 N44 113.6(11) . . ?
N39 C60 H60A 108.9 . . ?
N44 C60 H60A 108.8 . . ?
N39 C60 H60B 108.8 . . ?
N44 C60 H60B 108.8 . . ?
H60A C60 H60B 107.7 . . ?
O21 C61 N42 125.8(14) . . ?
O21 C61 N41 126.1(15) . . ?
N42 C61 N41 108.1(12) . . ?
C61 N41 C59 120.5(12) . . ?
C61 N41 C62 111.1(12) . . ?
C59 N41 C62 125.5(11) . . ?
C61 N42 C63 112.8(11) . . ?
C61 N42 C65 121.3(12) . . ?
C63 N42 C65 120.5(13) . . ?
N44 C62 N41 117.6(13) . . ?
N44 C62 C63 103.7(12) . . ?
N41 C62 C63 103.7(11) . . ?
N44 C62 H62 110.4 . . ?
N41 C62 H62 110.4 . . ?
C63 C62 H62 110.5 . . ?
N42 C63 N43 116.3(12) . . ?
N42 C63 C62 103.7(12) . . ?
N43 C63 C62 101.8(12) . . ?
N42 C63 H63 111.4 . . ?
N43 C63 H63 111.5 . . ?
C62 C63 H63 111.4 . . ?
C64 N43 C66 126.0(15) . . ?
C64 N43 C63 108.8(13) . . ?
C66 N43 C63 123.5(14) . . ?
C64 N44 C62 110.5(14) . . ?
C64 N44 C60 125.4(13) . . ?
C62 N44 C60 120.4(12) . . ?
N43 C64 N44 114.9(15) . . ?
N43 C64 O22 120.5(14) . . ?
N44 C64 O22 124.1(15) . . ?
N45 C65 N42 113.2(16) . . ?
N45 C65 H65A 109.0 . . ?
N42 C65 H65A 109.0 . . ?
N45 C65 H65B 108.9 . . ?
N42 C65 H65B 108.9 . . ?
H65A C65 H65B 107.7 . . ?
N43 C66 N48 114.2(12) . . ?
N43 C66 H66A 108.7 . . ?
N48 C66 H66A 108.7 . . ?
N43 C66 H66B 108.7 . . ?
N48 C66 H66B 108.7 . . ?
H66A C66 H66B 107.6 . . ?
O23 C67 N45 125.9(14) . . ?
O23 C67 N46 125.1(13) . . ?
N45 C67 N46 108.8(12) . . ?
C67 N45 C65 122.8(13) . . ?
C67 N45 C68 112.0(12) . . ?
C65 N45 C68 121.2(13) . . ?
C67 N46 C69 112.0(11) . . ?
C67 N46 C71 122.7(12) . . ?
C69 N46 C71 124.3(12) . . ?
N48 C68 N45 117.4(12) . . ?
N48 C68 C69 103.1(12) . . ?
N45 C68 C69 103.5(11) . . ?
N48 C68 H68 110.8 . . ?
N45 C68 H68 110.7 . . ?
C69 C68 H68 110.7 . . ?
N46 C69 N47 114.0(12) . . ?
N46 C69 C68 103.2(12) . . ?
N47 C69 C68 102.6(11) . . ?
N46 C69 H69 112.1 . . ?
N47 C69 H69 112.1 . . ?
C68 C69 H69 112.1 . . ?
C70 N47 C72 121.2(12) . . ?
C70 N47 C69 112.0(11) . . ?
C72 N47 C69 119.6(11) . . ?
C70 N48 C68 113.2(11) . . ?
C70 N48 C66 121.8(12) . . ?
C68 N48 C66 122.1(13) . . ?
O24 C70 N47 128.7(14) . . ?
O24 C70 N48 123.6(13) . . ?
N47 C70 N48 107.7(12) . . ?
N49 C71 N46 112.8(11) . . ?
N49 C71 H71A 109.0 . . ?
N46 C71 H71A 109.0 . . ?
N49 C71 H71B 109.0 . . ?
N46 C71 H71B 109.0 . . ?
H71A C71 H71B 107.8 . . ?
N52 C72 N47 112.3(11) . . ?
N52 C72 H72A 109.1 . . ?
N47 C72 H72A 109.1 . . ?
N52 C72 H72B 109.1 . . ?
N47 C72 H72B 109.2 . . ?
H72A C72 H72B 107.9 . . ?
O25 C73 N50 126.6(13) . . ?
O25 C73 N49 124.8(13) . . ?
N50 C73 N49 108.5(13) . . ?
C73 N49 C71 120.9(13) . . ?
C73 N49 C74 112.2(11) . . ?
C71 N49 C74 122.3(13) . . ?
C73 N50 C77 121.3(12) . . ?
C73 N50 C75 110.8(11) . . ?
C77 N50 C75 125.4(12) . . ?
N49 C74 N52 113.7(10) . . ?
N49 C74 C75 102.5(10) . . ?
N52 C74 C75 101.9(11) . . ?
N49 C74 H74 112.6 . . ?
N52 C74 H74 112.6 . . ?
C75 C74 H74 112.6 . . ?
N50 C75 N51 115.1(10) . . ?
N50 C75 C74 105.0(11) . . ?
N51 C75 C74 104.1(10) . . ?
N50 C75 H75 110.7 . . ?
N51 C75 H75 110.7 . . ?
C74 C75 H75 110.8 . . ?
C76 N51 C78 121.8(11) . . ?
C76 N51 C75 113.1(11) . . ?
C78 N51 C75 123.6(10) . . ?
C76 N52 C72 122.8(11) . . ?
C76 N52 C74 112.8(10) . . ?
C72 N52 C74 121.9(11) . . ?
O26 C76 N51 127.3(13) . . ?
O26 C76 N52 124.7(13) . . ?
N51 C76 N52 107.9(11) . . ?
N50 C77 N53 113.8(10) . . ?
N50 C77 H77A 108.8 . . ?
N53 C77 H77A 108.8 . . ?
N50 C77 H77B 108.8 . . ?
N53 C77 H77B 108.8 . . ?
H77A C77 H77B 107.7 . . ?
N51 C78 N56 114.3(11) . . ?
N51 C78 H78A 108.7 . . ?
N56 C78 H78A 108.7 . . ?
N51 C78 H78B 108.7 . . ?
N56 C78 H78B 108.7 . . ?
H78A C78 H78B 107.6 . . ?
O27 C79 N53 124.7(13) . . ?
O27 C79 N54 123.6(12) . . ?
N53 C79 N54 111.7(13) . . ?
C79 N53 C81 112.9(12) . . ?
C79 N53 C77 121.8(13) . . ?
C81 N53 C77 123.4(11) . . ?
C79 N54 C83 122.6(13) . . ?
C79 N54 C80 108.1(11) . . ?
C83 N54 C80 126.3(13) . . ?
N55 C80 N54 115.4(11) . . ?
N55 C80 C81 104.2(10) . . ?
N54 C80 C81 105.8(11) . . ?
N55 C80 H80 110.4 . . ?
N54 C80 H80 110.4 . . ?
C81 C80 H80 110.4 . . ?
N53 C81 N56 112.2(11) . . ?
N53 C81 C80 101.2(10) . . ?
N56 C81 C80 101.5(10) . . ?
N53 C81 H81 113.6 . . ?
N56 C81 H81 113.5 . . ?
C80 C81 H81 113.6 . . ?
C82 N55 C84 123.1(12) . . ?
C82 N55 C80 112.7(11) . . ?
C84 N55 C80 122.4(11) . . ?
C82 N56 C78 123.2(11) . . ?
C82 N56 C81 110.6(10) . . ?
C78 N56 C81 123.1(10) . . ?
O28 C82 N55 127.8(12) . . ?
O28 C82 N56 122.5(11) . . ?
N55 C82 N56 109.6(12) . . ?
N54 C83 N57 112.1(10) . . ?
N54 C83 H83A 109.3 . . ?
N57 C83 H83A 109.2 . . ?
N54 C83 H83B 109.1 . . ?
N57 C83 H83B 109.2 . . ?
H83A C83 H83B 107.9 . . ?
N55 C84 N60 116.5(13) . . ?
N55 C84 H84A 108.1 . . ?
N60 C84 H84A 108.2 . . ?
N55 C84 H84B 108.2 . . ?
N60 C84 H84B 108.2 . . ?
H84A C84 H84B 107.3 . . ?
O29 C85 N57 128.8(12) . . ?
O29 C85 N58 125.6(13) . . ?
N57 C85 N58 105.6(13) . . ?
C85 N57 C87 113.9(11) . . ?
C85 N57 C83 118.4(12) . . ?
C87 N57 C83 122.2(12) . . ?
C85 N58 C89 120.4(13) . . ?
C85 N58 C86 113.2(11) . . ?
C89 N58 C86 122.9(11) . . ?
N58 C86 N59 115.0(11) . . ?
N58 C86 C87 102.5(10) . . ?
N59 C86 C87 102.0(10) . . ?
N58 C86 H86 112.1 . . ?
N59 C86 H86 112.1 . . ?
C87 C86 H86 112.1 . . ?
N57 C87 N60 117.8(11) . . ?
N57 C87 C86 103.9(11) . . ?
N60 C87 C86 102.0(10) . . ?
N57 C87 H87 110.8 . . ?
N60 C87 H87 110.8 . . ?
C86 C87 H87 110.8 . . ?
C88 N59 C86 113.8(10) . . ?
C88 N59 C90 118.9(12) . . ?
C86 N59 C90 119.9(11) . . ?
C88 N60 C87 115.0(10) . . ?
C88 N60 C84 123.5(12) . . ?
C87 N60 C84 119.0(10) . . ?
O30 C88 N60 126.7(12) . . ?
O30 C88 N59 127.9(11) . . ?
N60 C88 N59 105.2(11) . . ?
N58 C89 N61 111.2(11) . . ?
N58 C89 H89A 109.4 . . ?
N61 C89 H89A 109.4 . . ?
N58 C89 H89B 109.4 . . ?
N61 C89 H89B 109.4 . . ?
H89A C89 H89B 108.0 . . ?
N64 C90 N59 115.4(12) . . ?
N64 C90 H90A 108.4 . . ?
N59 C90 H90A 108.4 . . ?
N64 C90 H90B 108.5 . . ?
N59 C90 H90B 108.4 . . ?
H90A C90 H90B 107.5 . . ?
O31 C91 N61 127.7(11) . . ?
O31 C91 N62 124.5(13) . . ?
N61 C91 N62 107.8(11) . . ?
C91 N61 C92 112.3(9) . . ?
C91 N61 C89 119.5(11) . . ?
C92 N61 C89 124.0(10) . . ?
C91 N62 C95 123.5(12) . . ?
C91 N62 C93 111.1(10) . . ?
C95 N62 C93 124.7(11) . . ?
N64 C92 N61 117.5(10) . . ?
N64 C92 C93 104.8(9) . . ?
N61 C92 C93 104.4(9) . . ?
N64 C92 H92 109.9 . . ?
N61 C92 H92 109.9 . . ?
C93 C92 H92 109.9 . . ?
N63 C93 N62 114.2(10) . . ?
N63 C93 C92 102.6(10) . . ?
N62 C93 C92 104.0(9) . . ?
N63 C93 H93 111.8 . . ?
N62 C93 H93 111.8 . . ?
C92 C93 H93 111.8 . . ?
C94 N63 C93 111.2(10) . . ?
C94 N63 C96 121.2(12) . . ?
C93 N63 C96 123.4(11) . . ?
C94 N64 C90 122.8(12) . . ?
C94 N64 C92 111.0(10) . . ?
C90 N64 C92 126.2(11) . . ?
O32 C94 N64 125.5(13) . . ?
O32 C94 N63 125.6(13) . . ?
N64 C94 N63 108.9(11) . . ?
N62 C95 N33 113.7(10) . . ?
N62 C95 H95A 108.8 . . ?
N33 C95 H95A 108.8 . . ?
N62 C95 H95B 108.8 . . ?
N33 C95 H95B 108.9 . . ?
H95A C95 H95B 107.7 . . ?
N63 C96 N36 112.8(10) . . ?
N63 C96 H96A 109.0 . . ?
N36 C96 H96A 109.1 . . ?
N63 C96 H96B 109.0 . . ?
N36 C96 H96B 109.0 . . ?
H96A C96 H96B 107.8 . . ?
N66 Pt1 N67 81.6(5) . . ?
N66 Pt1 N65 78.8(5) . . ?
N67 Pt1 N65 160.5(5) . . ?
N66 Pt1 Cl1 177.5(4) . . ?
N67 Pt1 Cl1 100.7(4) . . ?
N65 Pt1 Cl1 98.8(3) . . ?
C101 N65 C97 119.6(14) . . ?
C101 N65 Pt1 114.7(10) . . ?
C97 N65 Pt1 125.7(11) . . ?
C98 C97 N65 118.5(14) . . ?
C98 C97 H97 120.8 . . ?
N65 C97 H97 120.8 . . ?
C99 C98 C97 122.3(17) . . ?
C99 C98 H98 118.9 . . ?
C97 C98 H98 118.8 . . ?
C98 C99 C100 121.3(19) . . ?
C98 C99 H99 119.3 . . ?
C100 C99 H99 119.4 . . ?
C101 C100 C99 116.1(15) . . ?
C101 C100 H100 121.9 . . ?
C99 C100 H100 122.0 . . ?
N65 C101 C100 122.1(13) . . ?
N65 C101 C102 114.1(14) . . ?
C100 C101 C102 123.7(13) . . ?
N66 C102 C103 119.2(13) . . ?
N66 C102 C101 112.0(12) . . ?
C103 C102 C101 128.8(14) . . ?
C104 C103 C102 122.2(15) . . ?
C104 C103 H103 118.9 . . ?
C102 C103 H103 119.0 . . ?
C103 C104 C105 114.9(16) . . ?
C103 C104 C112 121.8(17) . . ?
C105 C104 C112 123.3(15) . . ?
C106 C105 C104 123.2(14) . . ?
C106 C105 H105 118.5 . . ?
C104 C105 H105 118.4 . . ?
C105 C106 N66 115.9(13) . . ?
C105 C106 C107 129.0(12) . . ?
N66 C106 C107 115.1(13) . . ?
C102 N66 C106 124.5(13) . . ?
C102 N66 Pt1 120.2(10) . . ?
C106 N66 Pt1 115.1(10) . . ?
N67 C107 C108 119.4(14) . . ?
N67 C107 C106 114.0(14) . . ?
C108 C107 C106 126.6(14) . . ?
C109 C108 C107 120.1(16) . . ?
C109 C108 H108 119.9 . . ?
C107 C108 H108 119.9 . . ?
C110 C109 C108 125.6(19) . . ?
C110 C109 H109 117.2 . . ?
C108 C109 H109 117.2 . . ?
C109 C110 C111 112.7(18) . . ?
C109 C110 H110 123.7 . . ?
C111 C110 H110 123.7 . . ?
N67 C111 C110 122.5(16) . . ?
N67 C111 H111 118.7 . . ?
C110 C111 H111 118.8 . . ?
C111 N67 C107 119.6(14) . . ?
C111 N67 Pt1 126.2(11) . . ?
C107 N67 Pt1 114.1(10) . . ?
C117 C112 C113 117.3(18) . . ?
C117 C112 C104 123.3(13) . . ?
C113 C112 C104 119.4(18) . . ?
C114 C113 C112 120.7(19) . . ?
C114 C113 H113 119.6 . . ?
C112 C113 H113 119.6 . . ?
C113 C114 C115 121.0(18) . . ?
C113 C114 H114 119.5 . . ?
C115 C114 H114 119.5 . . ?
C116 C115 C114 118.2(16) . . ?
C116 C115 C118 121.3(19) . . ?
C114 C115 C118 120.4(16) . . ?
C117 C116 C115 121.5(18) . . ?
C117 C116 H116 119.2 . . ?
C115 C116 H116 119.3 . . ?
C116 C117 C112 121.1(17) . . ?
C116 C117 H117 119.4 . . ?
C112 C117 H117 119.5 . . ?
C115 C118 H11C 109.5 . . ?
C115 C118 H11D 109.4 . . ?
H11C C118 H11D 109.5 . . ?
C115 C118 H11E 109.5 . . ?
H11C C118 H11E 109.5 . . ?
H11D C118 H11E 109.5 . . ?
N69 Pt2 N68 81.3(4) . . ?
N69 Pt2 N70 82.7(4) . . ?
N68 Pt2 N70 163.9(4) . . ?
N69 Pt2 Cl2 174.4(3) . . ?
N68 Pt2 Cl2 99.5(3) . . ?
N70 Pt2 Cl2 96.6(3) . . ?
C119 N68 C123 120.0(12) . . ?
C119 N68 Pt2 127.4(10) . . ?
C123 N68 Pt2 112.5(8) . . ?
N68 C119 C120 120.4(14) . . ?
N68 C119 H119 119.8 . . ?
C120 C119 H119 119.8 . . ?
C121 C120 C119 119.9(13) . . ?
C121 C120 H120 120.0 . . ?
C119 C120 H120 120.0 . . ?
C122 C121 C120 122.8(14) . . ?
C122 C121 H121 118.6 . . ?
C120 C121 H121 118.6 . . ?
C121 C122 C123 115.6(15) . . ?
C121 C122 H122 122.2 . . ?
C123 C122 H122 122.2 . . ?
N68 C123 C122 121.2(12) . . ?
N68 C123 C124 114.9(11) . . ?
C122 C123 C124 123.8(13) . . ?
N69 C124 C125 121.2(12) . . ?
N69 C124 C123 111.7(11) . . ?
C125 C124 C123 126.8(13) . . ?
C124 C125 C126 116.2(13) . . ?
C124 C125 H125 121.9 . . ?
C126 C125 H125 121.9 . . ?
C127 C126 C125 119.9(12) . . ?
C127 C126 C134 121.2(13) . . ?
C125 C126 C134 118.8(14) . . ?
C128 C127 C126 121.8(13) . . ?
C128 C127 H127 119.1 . . ?
C126 C127 H127 119.1 . . ?
C127 C128 N69 118.1(13) . . ?
C127 C128 C129 130.4(12) . . ?
N69 C128 C129 111.5(10) . . ?
C124 N69 C128 122.6(11) . . ?
C124 N69 Pt2 119.6(8) . . ?
C128 N69 Pt2 117.8(9) . . ?
C130 C129 N70 119.4(14) . . ?
C130 C129 C128 122.7(12) . . ?
N70 C129 C128 117.9(12) . . ?
C131 C130 C129 118.8(14) . . ?
C131 C130 H130 120.6 . . ?
C129 C130 H130 120.6 . . ?
C130 C131 C132 124.1(17) . . ?
C130 C131 H131 117.9 . . ?
C132 C131 H131 118.0 . . ?
C133 C132 C131 115.6(18) . . ?
C133 C132 H132 122.2 . . ?
C131 C132 H132 122.2 . . ?
N70 C133 C132 121.2(15) . . ?
N70 C133 H133 119.4 . . ?
C132 C133 H133 119.4 . . ?
C133 N70 C129 120.7(12) . . ?
C133 N70 Pt2 129.3(9) . . ?
C129 N70 Pt2 110.0(9) . . ?
C135 C134 C139 116.7(14) . . ?
C135 C134 C126 122.9(15) . . ?
C139 C134 C126 120.3(14) . . ?
C134 C135 C136 127.4(16) . . ?
C134 C135 H135 116.3 . . ?
C136 C135 H135 116.3 . . ?
C135 C136 C137 114.0(15) . . ?
C135 C136 H136 123.0 . . ?
C137 C136 H136 123.0 . . ?
C138 C137 C136 118.4(15) . . ?
C138 C137 C140 122(2) . . ?
C136 C137 C140 119.5(19) . . ?
C137 C138 C139 122.8(19) . . ?
C137 C138 H138 118.6 . . ?
C139 C138 H138 118.6 . . ?
C134 C139 C138 120.8(17) . . ?
C134 C139 H139 119.6 . . ?
C138 C139 H139 119.6 . . ?
C137 C140 H14A 109.5 . . ?
C137 C140 H14B 109.4 . . ?
H14A C140 H14B 109.5 . . ?
C137 C140 H14C 109.5 . . ?
H14A C140 H14C 109.5 . . ?
H14B C140 H14C 109.5 . . ?
N72 Pt3 N73 82.3(4) . . ?
N72 Pt3 N71 79.8(4) . . ?
N73 Pt3 N71 162.0(5) . . ?
N72 Pt3 Cl3 179.1(3) . . ?
N73 Pt3 Cl3 97.7(3) . . ?
N71 Pt3 Cl3 100.1(4) . . ?
C141 N71 C145 121.7(12) . . ?
C141 N71 Pt3 125.9(11) . . ?
C145 N71 Pt3 112.4(8) . . ?
N71 C141 C142 119.3(16) . . ?
N71 C141 H141 120.4 . . ?
C142 C141 H141 120.3 . . ?
C143 C142 C141 117.7(14) . . ?
C143 C142 H142 121.2 . . ?
C141 C142 H142 121.2 . . ?
C142 C143 C144 125.9(15) . . ?
C142 C143 H143 117.1 . . ?
C144 C143 H143 117.0 . . ?
C145 C144 C143 112.0(15) . . ?
C145 C144 H144 124.0 . . ?
C143 C144 H144 124.0 . . ?
N71 C145 C144 123.5(12) . . ?
N71 C145 C146 117.1(11) . . ?
C144 C145 C146 119.4(13) . . ?
N72 C146 C147 120.4(12) . . ?
N72 C146 C145 108.8(12) . . ?
C147 C146 C145 130.8(12) . . ?
C148 C147 C146 118.6(12) . . ?
C148 C147 H147 120.7 . . ?
C146 C147 H147 120.7 . . ?
C149 C148 C147 120.6(14) . . ?
C149 C148 C156 119.8(13) . . ?
C147 C148 C156 119.4(13) . . ?
C148 C149 C150 120.1(13) . . ?
C148 C149 H149 119.9 . . ?
C150 C149 H149 120.0 . . ?
N72 C150 C151 115.9(11) . . ?
N72 C150 C149 117.5(12) . . ?
C151 C150 C149 126.5(12) . . ?
C146 N72 C150 122.7(11) . . ?
C146 N72 Pt3 121.6(9) . . ?
C150 N72 Pt3 115.3(8) . . ?
C152 C151 C150 129.0(14) . . ?
C152 C151 N73 116.2(14) . . ?
C150 C151 N73 114.8(10) . . ?
C151 C152 C153 120.9(16) . . ?
C151 C152 H152 119.6 . . ?
C153 C152 H152 119.5 . . ?
C154 C153 C152 120.6(14) . . ?
C154 C153 H153 119.7 . . ?
C152 C153 H153 119.7 . . ?
C153 C154 C155 120.0(16) . . ?
C153 C154 H154 120.0 . . ?
C155 C154 H154 120.0 . . ?
N73 C155 C154 122.9(16) . . ?
N73 C155 H155 118.6 . . ?
C154 C155 H155 118.6 . . ?
C155 N73 C151 119.2(12) . . ?
C155 N73 Pt3 129.1(10) . . ?
C151 N73 Pt3 111.7(8) . . ?
C161 C156 C157 117.1(14) . . ?
C161 C156 C148 123.7(13) . . ?
C157 C156 C148 119.0(13) . . ?
C156 C157 C158 120.2(15) . . ?
C156 C157 H157 119.9 . . ?
C158 C157 H157 119.9 . . ?
C157 C158 C159 121.7(16) . . ?
C157 C158 H158 119.1 . . ?
C159 C158 H158 119.2 . . ?
C160 C159 C158 114.0(15) . . ?
C160 C159 C162 123.0(17) . . ?
C158 C159 C162 122.9(19) . . ?
C161 C160 C159 123.2(15) . . ?
C161 C160 H160 118.4 . . ?
C159 C160 H160 118.4 . . ?
C156 C161 C160 123.7(15) . . ?
C156 C161 H161 118.2 . . ?
C160 C161 H161 118.2 . . ?
C159 C162 H16A 109.4 . . ?
C159 C162 H16B 109.5 . . ?
H16A C162 H16B 109.5 . . ?
C159 C162 H16C 109.5 . . ?
H16A C162 H16C 109.5 . . ?
H16B C162 H16C 109.5 . . ?
N75 Pt4 N76 82.3(5) . . ?
N75 Pt4 N74 80.6(5) . . ?
N76 Pt4 N74 163.0(5) . . ?
N75 Pt4 Cl4 177.2(4) . . ?
N76 Pt4 Cl4 100.4(4) . . ?
N74 Pt4 Cl4 96.6(4) . . ?
C167 N74 C163 122.8(15) . . ?
C167 N74 Pt4 113.9(10) . . ?
C163 N74 Pt4 123.2(12) . . ?
N74 C163 C164 117.7(19) . . ?
N74 C163 H163 121.2 . . ?
C164 C163 H163 121.1 . . ?
C165 C164 C163 119.7(17) . . ?
C165 C164 H164 120.1 . . ?
C163 C164 H164 120.1 . . ?
C164 C165 C166 119.1(18) . . ?
C164 C165 H165 120.5 . . ?
C166 C165 H165 120.5 . . ?
C167 C166 C165 116.0(17) . . ?
C167 C166 H166 122.0 . . ?
C165 C166 H166 122.0 . . ?
N74 C167 C166 124.0(14) . . ?
N74 C167 C168 113.9(14) . . ?
C166 C167 C168 121.9(16) . . ?
N75 C168 C169 120.3(13) . . ?
N75 C168 C167 112.8(14) . . ?
C169 C168 C167 126.8(13) . . ?
C170 C169 C168 119.0(13) . . ?
C170 C169 H169 120.5 . . ?
C168 C169 H169 120.5 . . ?
C171 C170 C169 124.4(14) . . ?
C171 C170 C178 114.2(12) . . ?
C169 C170 C178 121.3(13) . . ?
C170 C171 C172 113.1(13) . . ?
C170 C171 H171 123.5 . . ?
C172 C171 H171 123.5 . . ?
N75 C172 C173 113.3(15) . . ?
N75 C172 C171 121.2(13) . . ?
C173 C172 C171 125.5(14) . . ?
C172 N75 C168 121.9(14) . . ?
C172 N75 Pt4 119.3(11) . . ?
C168 N75 Pt4 118.8(10) . . ?
N76 C173 C174 120.1(17) . . ?
N76 C173 C172 114.7(15) . . ?
C174 C173 C172 125.2(17) . . ?
C175 C174 C173 117.6(18) . . ?
C175 C174 H174 121.2 . . ?
C173 C174 H174 121.2 . . ?
C174 C175 C176 121.3(18) . . ?
C174 C175 H175 119.3 . . ?
C176 C175 H175 119.4 . . ?
C177 C176 C175 116(2) . . ?
C177 C176 H176 121.8 . . ?
C175 C176 H176 121.9 . . ?
N76 C177 C176 125(2) . . ?
N76 C177 H177 117.3 . . ?
C176 C177 H177 117.4 . . ?
C177 N76 C173 119.2(16) . . ?
C177 N76 Pt4 130.2(13) . . ?
C173 N76 Pt4 110.4(11) . . ?
C179 C178 C183 119.8(15) . . ?
C179 C178 C170 122.4(14) . . ?
C183 C178 C170 117.8(14) . . ?
C180 C179 C178 121.3(16) . . ?
C180 C179 H179 119.4 . . ?
C178 C179 H179 119.3 . . ?
C179 C180 C181 123.0(16) . . ?
C179 C180 H180 118.5 . . ?
C181 C180 H180 118.5 . . ?
C180 C181 C182 116.8(16) . . ?
C180 C181 C184 123.6(17) . . ?
C182 C181 C184 119.5(18) . . ?
C181 C182 C183 119.8(17) . . ?
C181 C182 H182 120.1 . . ?
C183 C182 H182 120.1 . . ?
C178 C183 C182 119.1(17) . . ?
C178 C183 H183 120.5 . . ?
C182 C183 H183 120.4 . . ?
C181 C184 H18C 109.5 . . ?
C181 C184 H18D 109.4 . . ?
H18C C184 H18D 109.5 . . ?
C181 C184 H18E 109.5 . . ?
H18C C184 H18E 109.5 . . ?
H18D C184 H18E 109.5 . . ?
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
O1 C1 1.187(17) . ?
C1 N2 1.382(19) . ?
C1 N1 1.397(17) . ?
N1 C47 1.397(19) . ?
N1 C2 1.437(19) . ?
N2 C3 1.435(18) . ?
N2 C5 1.467(18) . ?
C2 N4 1.421(17) . ?
C2 C3 1.53(2) . ?
C2 H2 1.0000 . ?
C3 N3 1.447(17) . ?
C3 H3 1.0000 . ?
N3 C4 1.32(2) . ?
N3 C6 1.468(19) . ?
N4 C4 1.36(2) . ?
N4 C48 1.473(16) . ?
C4 O2 1.268(18) . ?
C5 N5 1.42(2) . ?
C5 H5A 0.9900 . ?
C5 H5B 0.9900 . ?
C6 N8 1.440(18) . ?
C6 H6A 0.9900 . ?
C6 H6B 0.9900 . ?
C7 O3 1.231(17) . ?
C7 N6 1.376(19) . ?
C7 N5 1.395(19) . ?
N5 C8 1.419(19) . ?
N6 C11 1.442(16) . ?
N6 C9 1.465(18) . ?
C8 N8 1.448(16) . ?
C8 C9 1.54(2) . ?
C8 H8 1.0000 . ?
C9 N7 1.435(15) . ?
C9 H9 1.0000 . ?
N7 C10 1.350(17) . ?
N7 C12 1.462(18) . ?
N8 C10 1.412(18) . ?
C10 O4 1.203(15) . ?
C11 N9 1.396(17) . ?
C11 H11A 0.9900 . ?
C11 H11B 0.9900 . ?
C12 N12 1.448(17) . ?
C12 H12A 0.9900 . ?
C12 H12B 0.9900 . ?
C13 O5 1.241(15) . ?
C13 N10 1.327(18) . ?
C13 N9 1.376(16) . ?
N9 C14 1.486(16) . ?
N10 C17 1.408(17) . ?
N10 C15 1.435(16) . ?
C14 N12 1.449(15) . ?
C14 C15 1.558(18) . ?
C14 H14 1.0000 . ?
C15 N11 1.409(16) . ?
C15 H15 1.0000 . ?
N11 C16 1.376(17) . ?
N11 C18 1.453(17) . ?
N12 C16 1.337(16) . ?
C16 O6 1.233(14) . ?
C17 N13 1.448(16) . ?
C17 H17A 0.9900 . ?
C17 H17B 0.9900 . ?
C18 N16 1.465(16) . ?
C18 H18A 0.9900 . ?
C18 H18B 0.9900 . ?
C19 O7 1.197(16) . ?
C19 N14 1.375(17) . ?
C19 N13 1.383(18) . ?
N13 C20 1.440(18) . ?
N14 C21 1.425(18) . ?
N14 C23 1.438(18) . ?
C20 N16 1.471(15) . ?
C20 C21 1.546(18) . ?
C20 H20 1.0000 . ?
C21 N15 1.483(16) . ?
C21 H21 1.0000 . ?
N15 C22 1.335(16) . ?
N15 C24 1.474(16) . ?
N16 C22 1.382(17) . ?
C22 O8 1.226(14) . ?
C23 N17 1.452(19) . ?
C23 H23A 0.9900 . ?
C23 H23B 0.9900 . ?
C24 N20 1.44(2) . ?
C24 H24A 0.9900 . ?
C24 H24B 0.9900 . ?
C25 O9 1.211(17) . ?
C25 N18 1.364(17) . ?
C25 N17 1.40(2) . ?
N17 C26 1.406(18) . ?
N18 C29 1.46(2) . ?
N18 C27 1.478(19) . ?
C26 N20 1.462(16) . ?
C26 C27 1.52(2) . ?
C26 H26 1.0000 . ?
C27 N19 1.414(17) . ?
C27 H27 1.0000 . ?
N19 C30 1.448(17) . ?
N19 C28 1.448(18) . ?
N20 C28 1.470(19) . ?
C28 O10 1.179(15) . ?
C29 N21 1.449(17) . ?
C29 H29A 0.9900 . ?
C29 H29B 0.9900 . ?
C30 N24 1.431(18) . ?
C30 H30A 0.9900 . ?
C30 H30B 0.9900 . ?
C31 O11 1.235(14) . ?
C31 N21 1.330(17) . ?
C31 N22 1.359(16) . ?
N21 C32 1.410(16) . ?
N22 C35 1.42(2) . ?
N22 C33 1.479(16) . ?
C32 N24 1.434(18) . ?
C32 C33 1.60(2) . ?
C32 H32 1.0000 . ?
C33 N23 1.444(17) . ?
C33 H33 1.0000 . ?
N23 C34 1.364(19) . ?
N23 C36 1.455(14) . ?
N24 C34 1.381(18) . ?
C34 O12 1.228(16) . ?
C35 N25 1.461(18) . ?
C35 H35A 0.9900 . ?
C35 H35B 0.9900 . ?
C36 N28 1.395(11) . ?
C36 H36A 0.9900 . ?
C36 H36B 0.9900 . ?
C37 O13 1.208(15) . ?
C37 N25 1.355(16) . ?
C37 N26 1.386(16) . ?
N25 C38 1.398(18) . ?
N26 C41 1.457(17) . ?
N26 C39 1.461(16) . ?
C38 N28 1.53(2) . ?
C38 C39 1.609(17) . ?
C38 H38 1.0000 . ?
C39 N27 1.419(19) . ?
C39 H39 1.0000 . ?
N27 C40 1.358(18) . ?
N27 C42 1.458(15) . ?
N28 C40 1.452(16) . ?
C40 O14 1.188(17) . ?
C41 N29 1.423(17) . ?
C41 H41A 0.9900 . ?
C41 H41B 0.9900 . ?
C42 N32 1.429(16) . ?
C42 H42A 0.9900 . ?
C42 H42B 0.9900 . ?
C43 O15 1.213(15) . ?
C43 N30 1.359(17) . ?
C43 N29 1.399(15) . ?
N29 C44 1.435(17) . ?
N30 C47 1.468(16) . ?
N30 C45 1.519(15) . ?
C44 N32 1.478(18) . ?
C44 C45 1.496(17) . ?
C44 H44 1.0000 . ?
C45 N31 1.435(17) . ?
C45 H45 1.0000 . ?
N31 C46 1.345(16) . ?
N31 C48 1.457(17) . ?
N32 C46 1.367(18) . ?
C46 O16 1.246(16) . ?
C47 H47A 0.9900 . ?
C47 H47B 0.9900 . ?
C48 H48A 0.9900 . ?
C48 H48B 0.9900 . ?
C49 O17 1.242(18) . ?
C49 N33 1.357(19) . ?
C49 N34 1.367(17) . ?
N33 C95 1.433(13) . ?
N33 C50 1.494(17) . ?
N34 C53 1.431(18) . ?
N34 C51 1.435(17) . ?
C50 N36 1.480(18) . ?
C50 C51 1.566(18) . ?
C50 H50 1.0000 . ?
C51 N35 1.456(19) . ?
C51 H51 1.0000 . ?
N35 C52 1.364(18) . ?
N35 C54 1.386(13) . ?
N36 C52 1.318(17) . ?
N36 C96 1.459(13) . ?
C52 O18 1.256(17) . ?
C53 N37 1.439(18) . ?
C53 H53A 0.9900 . ?
C53 H53B 0.9900 . ?
C54 N40 1.518(13) . ?
C54 H54A 0.9900 . ?
C54 H54B 0.9900 . ?
C55 O19 1.233(15) . ?
C55 N37 1.372(16) . ?
C55 N38 1.379(16) . ?
N37 C56 1.444(17) . ?
N38 C57 1.443(16) . ?
N38 C59 1.495(19) . ?
C56 N40 1.501(19) . ?
C56 C57 1.56(2) . ?
C56 H56 1.0000 . ?
C57 N39 1.449(19) . ?
C57 H57 1.0000 . ?
N39 C58 1.375(19) . ?
N39 C60 1.461(19) . ?
N40 C58 1.37(2) . ?
C58 O20 1.245(18) . ?
C59 N41 1.411(19) . ?
C59 H59A 0.9900 . ?
C59 H59B 0.9900 . ?
C60 N44 1.461(18) . ?
C60 H60A 0.9900 . ?
C60 H60B 0.9900 . ?
C61 O21 1.222(17) . ?
C61 N42 1.339(19) . ?
C61 N41 1.403(17) . ?
N41 C62 1.452(18) . ?
N42 C63 1.453(17) . ?
N42 C65 1.47(2) . ?
C62 N44 1.45(2) . ?
C62 C63 1.53(2) . ?
C62 H62 1.0000 . ?
C63 N43 1.52(2) . ?
C63 H63 1.0000 . ?
N43 C64 1.29(2) . ?
N43 C66 1.41(2) . ?
N44 C64 1.301(19) . ?
C64 O22 1.314(19) . ?
C65 N45 1.43(2) . ?
C65 H65A 0.9900 . ?
C65 H65B 0.9900 . ?
C66 N48 1.462(18) . ?
C66 H66A 0.9900 . ?
C66 H66B 0.9900 . ?
C67 O23 1.241(17) . ?
C67 N45 1.333(18) . ?
C67 N46 1.393(19) . ?
N45 C68 1.450(19) . ?
N46 C69 1.421(19) . ?
N46 C71 1.484(17) . ?
C68 N48 1.442(17) . ?
C68 C69 1.55(2) . ?
C68 H68 1.0000 . ?
C69 N47 1.490(19) . ?
C69 H69 1.0000 . ?
N47 C70 1.348(17) . ?
N47 C72 1.463(16) . ?
N48 C70 1.392(18) . ?
C70 O24 1.211(17) . ?
C71 N49 1.403(19) . ?
C71 H71A 0.9900 . ?
C71 H71B 0.9900 . ?
C72 N52 1.427(16) . ?
C72 H72A 0.9900 . ?
C72 H72B 0.9900 . ?
C73 O25 1.259(18) . ?
C73 N50 1.356(18) . ?
C73 N49 1.387(18) . ?
N49 C74 1.422(18) . ?
N50 C77 1.424(16) . ?
N50 C75 1.433(17) . ?
C74 N52 1.487(15) . ?
C74 C75 1.546(18) . ?
C74 H74 1.0000 . ?
C75 N51 1.463(16) . ?
C75 H75 1.0000 . ?
N51 C76 1.358(17) . ?
N51 C78 1.433(16) . ?
N52 C76 1.379(17) . ?
C76 O26 1.223(16) . ?
C77 N53 1.469(17) . ?
C77 H77A 0.9900 . ?
C77 H77B 0.9900 . ?
C78 N56 1.463(15) . ?
C78 H78A 0.9900 . ?
C78 H78B 0.9900 . ?
C79 O27 1.248(17) . ?
C79 N53 1.335(17) . ?
C79 N54 1.362(18) . ?
N53 C81 1.454(19) . ?
N54 C83 1.421(16) . ?
N54 C80 1.471(19) . ?
C80 N55 1.417(17) . ?
C80 C81 1.547(17) . ?
C80 H80 1.0000 . ?
C81 N56 1.463(16) . ?
C81 H81 1.0000 . ?
N55 C82 1.321(16) . ?
N55 C84 1.413(19) . ?
N56 C82 1.361(17) . ?
C82 O28 1.263(16) . ?
C83 N57 1.460(16) . ?
C83 H83A 0.9900 . ?
C83 H83B 0.9900 . ?
C84 N60 1.445(15) . ?
C84 H84A 0.9900 . ?
C84 H84B 0.9900 . ?
C85 O29 1.203(17) . ?
C85 N57 1.393(18) . ?
C85 N58 1.415(17) . ?
N57 C87 1.405(18) . ?
N58 C89 1.422(17) . ?
N58 C86 1.429(19) . ?
C86 N59 1.439(16) . ?
C86 C87 1.588(17) . ?
C86 H86 1.0000 . ?
C87 N60 1.442(17) . ?
C87 H87 1.0000 . ?
N59 C88 1.393(17) . ?
N59 C90 1.445(15) . ?
N60 C88 1.371(15) . ?
C88 O30 1.158(16) . ?
C89 N61 1.461(15) . ?
C89 H89A 0.9900 . ?
C89 H89B 0.9900 . ?
C90 N64 1.392(18) . ?
C90 H90A 0.9900 . ?
C90 H90B 0.9900 . ?
C91 O31 1.198(16) . ?
C91 N61 1.383(18) . ?
C91 N62 1.407(15) . ?
N61 C92 1.448(12) . ?
N62 C95 1.432(13) . ?
N62 C93 1.465(18) . ?
C92 N64 1.410(13) . ?
C92 C93 1.535(16) . ?
C92 H92 1.0000 . ?
C93 N63 1.443(16) . ?
C93 H93 1.0000 . ?
N63 C94 1.369(17) . ?
N63 C96 1.453(12) . ?
N64 C94 1.367(16) . ?
C94 O32 1.214(16) . ?
C95 H95A 0.9900 . ?
C95 H95B 0.9900 . ?
C96 H96A 0.9900 . ?
C96 H96B 0.9900 . ?
Pt1 N66 1.946(12) . ?
Pt1 N67 2.010(13) . ?
Pt1 N65 2.015(12) . ?
Pt1 Cl1 2.300(3) . ?
N65 C101 1.347(18) . ?
N65 C97 1.390(17) . ?
C97 C98 1.37(2) . ?
C97 H97 0.9500 . ?
C98 C99 1.31(2) . ?
C98 H98 0.9500 . ?
C99 C100 1.41(2) . ?
C99 H99 0.9500 . ?
C100 C101 1.39(2) . ?
C100 H100 0.9500 . ?
C101 C102 1.48(2) . ?
C102 N66 1.301(18) . ?
C102 C103 1.395(19) . ?
C103 C104 1.39(2) . ?
C103 H103 0.9500 . ?
C104 C105 1.43(2) . ?
C104 C112 1.46(3) . ?
C105 C106 1.378(19) . ?
C105 H105 0.9500 . ?
C106 N66 1.391(17) . ?
C106 C107 1.44(2) . ?
C107 N67 1.377(18) . ?
C107 C108 1.39(2) . ?
C108 C109 1.35(3) . ?
C108 H108 0.9500 . ?
C109 C110 1.33(3) . ?
C109 H109 0.9500 . ?
C110 C111 1.51(3) . ?
C110 H110 0.9500 . ?
C111 N67 1.332(19) . ?
C111 H111 0.9500 . ?
C112 C117 1.36(2) . ?
C112 C113 1.43(2) . ?
C113 C114 1.31(2) . ?
C113 H113 0.9500 . ?
C114 C115 1.38(3) . ?
C114 H114 0.9500 . ?
C115 C116 1.38(2) . ?
C115 C118 1.57(2) . ?
C116 C117 1.34(2) . ?
C116 H116 0.9500 . ?
C117 H117 0.9500 . ?
C118 H11C 0.9800 . ?
C118 H11D 0.9800 . ?
C118 H11E 0.9800 . ?
Pt2 N69 1.928(10) . ?
Pt2 N68 2.014(11) . ?
Pt2 N70 2.034(11) . ?
Pt2 Cl2 2.293(3) . ?
N68 C119 1.339(15) . ?
N68 C123 1.383(16) . ?
C119 C120 1.38(2) . ?
C119 H119 0.9500 . ?
C120 C121 1.37(2) . ?
C120 H120 0.9500 . ?
C121 C122 1.37(2) . ?
C121 H121 0.9500 . ?
C122 C123 1.43(2) . ?
C122 H122 0.9500 . ?
C123 C124 1.495(17) . ?
C124 N69 1.325(17) . ?
C124 C125 1.403(17) . ?
C125 C126 1.414(19) . ?
C125 H125 0.9500 . ?
C126 C127 1.38(2) . ?
C126 C134 1.468(18) . ?
C127 C128 1.344(17) . ?
C127 H127 0.9500 . ?
C128 N69 1.375(15) . ?
C128 C129 1.46(2) . ?
C129 C130 1.394(18) . ?
C129 N70 1.393(16) . ?
C130 C131 1.32(2) . ?
C130 H130 0.9500 . ?
C131 C132 1.43(2) . ?
C131 H131 0.9500 . ?
C132 C133 1.39(3) . ?
C132 H132 0.9500 . ?
C133 N70 1.363(18) . ?
C133 H133 0.9500 . ?
C134 C135 1.32(2) . ?
C134 C139 1.38(2) . ?
C135 C136 1.40(2) . ?
C135 H135 0.9500 . ?
C136 C137 1.49(3) . ?
C136 H136 0.9500 . ?
C137 C138 1.33(3) . ?
C137 C140 1.53(2) . ?
C138 C139 1.39(2) . ?
C138 H138 0.9500 . ?
C139 H139 0.9500 . ?
C140 H14A 0.9800 . ?
C140 H14B 0.9800 . ?
C140 H14C 0.9800 . ?
Pt3 N72 1.957(11) . ?
Pt3 N73 1.989(9) . ?
Pt3 N71 2.044(10) . ?
Pt3 Cl3 2.288(4) . ?
N71 C141 1.337(16) . ?
N71 C145 1.365(17) . ?
C141 C142 1.43(2) . ?
C141 H141 0.9500 . ?
C142 C143 1.34(2) . ?
C142 H142 0.9500 . ?
C143 C144 1.43(2) . ?
C143 H143 0.9500 . ?
C144 C145 1.409(18) . ?
C144 H144 0.9500 . ?
C145 C146 1.514(18) . ?
C146 N72 1.328(16) . ?
C146 C147 1.38(2) . ?
C147 C148 1.381(18) . ?
C147 H147 0.9500 . ?
C148 C149 1.35(2) . ?
C148 C156 1.50(2) . ?
C149 C150 1.409(19) . ?
C149 H149 0.9500 . ?
C150 N72 1.360(15) . ?
C150 C151 1.398(19) . ?
C151 C152 1.374(17) . ?
C151 N73 1.438(17) . ?
C152 C153 1.38(2) . ?
C152 H152 0.9500 . ?
C153 C154 1.30(2) . ?
C153 H153 0.9500 . ?
C154 C155 1.36(2) . ?
C154 H154 0.9500 . ?
C155 N73 1.299(17) . ?
C155 H155 0.9500 . ?
C156 C161 1.35(2) . ?
C156 C157 1.403(19) . ?
C157 C158 1.42(2) . ?
C157 H157 0.9500 . ?
C158 C159 1.44(3) . ?
C158 H158 0.9500 . ?
C159 C160 1.39(2) . ?
C159 C162 1.47(2) . ?
C160 C161 1.37(2) . ?
C160 H160 0.9500 . ?
C161 H161 0.9500 . ?
C162 H16A 0.9800 . ?
C162 H16B 0.9800 . ?
C162 H16C 0.9800 . ?
Pt4 N75 1.890(13) . ?
Pt4 N76 2.006(14) . ?
Pt4 N74 2.071(13) . ?
Pt4 Cl4 2.303(4) . ?
N74 C167 1.30(2) . ?
N74 C163 1.336(19) . ?
C163 C164 1.42(3) . ?
C163 H163 0.9500 . ?
C164 C165 1.40(3) . ?
C164 H164 0.9500 . ?
C165 C166 1.42(2) . ?
C165 H165 0.9500 . ?
C166 C167 1.38(2) . ?
C166 H166 0.9500 . ?
C167 C168 1.52(2) . ?
C168 N75 1.347(18) . ?
C168 C169 1.37(2) . ?
C169 C170 1.355(17) . ?
C169 H169 0.9500 . ?
C170 C171 1.357(19) . ?
C170 C178 1.568(19) . ?
C171 C172 1.50(2) . ?
C171 H171 0.9500 . ?
C172 N75 1.293(19) . ?
C172 C173 1.47(2) . ?
C173 N76 1.39(2) . ?
C173 C174 1.41(2) . ?
C174 C175 1.40(3) . ?
C174 H174 0.9500 . ?
C175 C176 1.41(3) . ?
C175 H175 0.9500 . ?
C176 C177 1.36(3) . ?
C176 H176 0.9500 . ?
C177 N76 1.31(2) . ?
C177 H177 0.9500 . ?
C178 C179 1.38(2) . ?
C178 C183 1.40(2) . ?
C179 C180 1.36(2) . ?
C179 H179 0.9500 . ?
C180 C181 1.40(2) . ?
C180 H180 0.9500 . ?
C181 C182 1.43(3) . ?
C181 C184 1.50(2) . ?
C182 C183 1.44(3) . ?
C182 H182 0.9500 . ?
C183 H183 0.9500 . ?
C184 H18C 0.9800 . ?
C184 H18D 0.9800 . ?
C184 H18E 0.9800 . ?
