Information card for entry 1566535

Structure parameters

• Formula: C77 H110 Ga2 N8 Sb2
• Calculated formula: C77 H110 Ga2 N8 Sb2
• SMILES: [Sb]1([Sb][Ga]2(N(C(=CC(=[N]2c2c(cccc2C(C)C)C(C)C)C)C)c2c(cccc2C(C)C)C(C)C)N(C)C)[N](C)(C)[Ga]2(N(C(=CC(=[N]2c2c(cccc2C(C)C)C(C)C)C)C)c2c(cccc2C(C)C)C(C)C)N1c1ccccc1.c1(ccccc1)C.C(#N)C
• Title of publication: Synthesis of Distibiranes and Azadistibiranes by Cycloaddition Reactions of Distibenes with Diazomethanes and Azides
• Authors of publication: Weinert, Hanns Micha; Wölper, Christoph; Schulz, Stephan
• Journal of publication: Chemical Science
• Year of publication: 2022
• a: 13.6969 ± 0.0016 Å
• b: 28.763 ± 0.003 Å
• c: 20.711 ± 0.003 Å
• α: 90°
• β: 94.587 ± 0.005°
• γ: 90°
• Cell volume: 8133.3 ± 1.7 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0462
• Residual factor for significantly intense reflections: 0.0299
• Weighted residual factors for significantly intense reflections: 0.0674
• Weighted residual factors for all reflections included in the refinement: 0.0752
• Goodness-of-fit parameter for all reflections included in the refinement: 1.06
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No