Information card for entry 1569240

Structure parameters

• Formula: C144 H120 As8 Au13 Cl4
• Calculated formula: C144 H120 As8 Au13 Cl4
• Title of publication: Monoarsine-protected icosahedral cluster [Au₁₃(AsPh₃)₈Cl₄]⁺: comparative studies on ligand effect and surface reactivity with its stibine analogue.
• Authors of publication: Yu, Jiu-Hong; Yuan, Zhi-Rui; Xu, Jing; Wang, Jin-Gui; Azam, Mohammad; Li, Tian-Duo; Li, Ying-Zhou; Sun, Di
• Journal of publication: Chemical science
• Year of publication: 2023
• Journal volume: 14
• Journal issue: 24
• Pages of publication: 6564 - 6571
• a: 28.1786 ± 0.0002 Å
• b: 31.8205 ± 0.0004 Å
• c: 36.1804 ± 0.0005 Å
• α: 90°
• β: 91.8449 ± 0.001°
• γ: 90°
• Cell volume: 32424.6 ± 0.6 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.1543
• Residual factor for significantly intense reflections: 0.1337
• Weighted residual factors for significantly intense reflections: 0.3421
• Weighted residual factors for all reflections included in the refinement: 0.3562
• Goodness-of-fit parameter for all reflections included in the refinement: 1.077
• Diffraction radiation wavelength: 1.54184 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No