Information card for entry 1571349

Structure parameters

• Formula: C88 H128 Ce K O15.5 Si4
• Calculated formula: C87.9996 H127.999 Ce K O15.4999 Si4
• Title of publication: Siloxide tripodal ligands as a scaffold for stabilizing lanthanides in the +4 oxidation state.
• Authors of publication: Tricoire, Maxime; Hsueh, Fang-Che; Keener, Megan; Rajeshkumar, Thayalan; Scopelliti, Rosario; Zivkovic, Ivica; Maron, Laurent; Mazzanti, Marinella
• Journal of publication: Chemical science
• Year of publication: 2024
• Journal volume: 15
• Journal issue: 18
• Pages of publication: 6874 - 6883
• a: 14.87393 ± 0.00016 Å
• b: 14.87393 ± 0.00016 Å
• c: 55.4259 ± 0.0007 Å
• α: 90°
• β: 90°
• γ: 120°
• Cell volume: 10619.3 ± 0.2 ų
• Cell temperature: 200 ± 0.11 K
• Ambient diffraction temperature: 200 ± 0.11 K
• Number of distinct elements: 6
• Space group number: 182
• Hermann-Mauguin space group symbol: P 63 2 2
• Hall space group symbol: P 6c 2c
• Residual factor for all reflections: 0.0588
• Residual factor for significantly intense reflections: 0.0581
• Weighted residual factors for significantly intense reflections: 0.1554
• Weighted residual factors for all reflections included in the refinement: 0.1561
• Goodness-of-fit parameter for all reflections included in the refinement: 1.088
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 1.54184 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No