Information card for entry 1572015

Structure parameters

• Formula: C35 H41 N3 O4 Si
• Calculated formula: C35 H41 N3 O4 Si
• Title of publication: Photoinduced [4 + 2]-cycloaddition reactions of vinyldiazo compounds for the construction of heterocyclic and bicyclic rings.
• Authors of publication: Bao, Ming; Bohórquez, Arnold R Romero; Arman, Hadi; Doyle, Michael P.
• Journal of publication: Chemical science
• Year of publication: 2024
• Journal volume: 15
• Journal issue: 30
• Pages of publication: 12042 - 12046
• a: 14.0714 ± 0.0002 Å
• b: 14.8588 ± 0.0002 Å
• c: 16.3784 ± 0.0002 Å
• α: 90.572 ± 0.001°
• β: 92.785 ± 0.001°
• γ: 107.376 ± 0.001°
• Cell volume: 3263.25 ± 0.08 ų
• Cell temperature: 100 ± 0.1 K
• Ambient diffraction temperature: 100 ± 0.1 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0737
• Residual factor for significantly intense reflections: 0.0669
• Weighted residual factors for significantly intense reflections: 0.1395
• Weighted residual factors for all reflections included in the refinement: 0.1432
• Goodness-of-fit parameter for all reflections included in the refinement: 1.002
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 1.54184 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No