Information card for entry 1572729

Structure parameters

• Formula: C207 H205 Cu9 N2 Na4 O49.5 P4 Si20
• Calculated formula: C207 H205 Cu9 N2 Na4 O49.5 P4 Si20
• Title of publication: An ionic Cu₉Na₄-phenylsilsesquioxane/bis(triphenylphosphine)iminium complex: synthesis, unique structure, and catalytic activity.
• Authors of publication: Bilyachenko, Alexey N.; Khrustalev, Victor N.; Huang, Zhibin; Dubinina, Kristina D.; Shubina, Elena S.; Lobanov, Nikolai N.; Sun, Di; Alegria, Elisabete C. B. A.; Pombeiro, Armando J. L.
• Journal of publication: Nanoscale
• Year of publication: 2024
• Journal volume: 16
• Journal issue: 41
• Pages of publication: 19266 - 19275
• a: 16.3354 ± 0.0009 Å
• b: 24.6172 ± 0.0013 Å
• c: 28.7146 ± 0.0015 Å
• α: 75.3941 ± 0.0012°
• β: 87.8609 ± 0.0013°
• γ: 89.5919 ± 0.0012°
• Cell volume: 11166.1 ± 1 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 8
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1898
• Residual factor for significantly intense reflections: 0.1034
• Weighted residual factors for significantly intense reflections: 0.2066
• Weighted residual factors for all reflections included in the refinement: 0.2383
• Goodness-of-fit parameter for all reflections included in the refinement: 1.059
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No