Information card for entry 1575003

Structure parameters

• Formula: C24 H16 Cl2 Mn N4
• Calculated formula: C24 H16 Cl2 Mn N4
• Title of publication: Manganese-mediated C(sp)-Si cross-electrophile coupling of alkynyl halides with chlorosilanes.
• Authors of publication: Lin, Quan; Lin, Liping; Wang, Jingjing; Yu, Daohong; Chen, Zhengwang; Wang, Zhong-Xia
• Journal of publication: Chemical science
• Year of publication: 2025
• Journal volume: 16
• Journal issue: 31
• Pages of publication: 14216 - 14224
• a: 10.2331 ± 0.0006 Å
• b: 17.097 ± 0.001 Å
• c: 12.6421 ± 0.0007 Å
• α: 90°
• β: 100.465 ± 0.005°
• γ: 90°
• Cell volume: 2175 ± 0.2 ų
• Cell temperature: 299.99 ± 0.1 K
• Ambient diffraction temperature: 299.99 ± 0.1 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.1676
• Residual factor for significantly intense reflections: 0.1305
• Weighted residual factors for significantly intense reflections: 0.3044
• Weighted residual factors for all reflections included in the refinement: 0.3278
• Goodness-of-fit parameter for all reflections included in the refinement: 1.036
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 1.54184 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No