Crystallography Open Database

Information card for entry 1575049

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Coordinates	1575049.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C152 H132 N4 O20 S4
Calculated formula	C152 H132 N4 O20 S4
Title of publication	Palladium-catalyzed redox diversified entry to axially chiral styrenes <i>via</i> asymmetric olefination with alkynes.
Authors of publication	Lin, Ziwei; Jiang, Yuqing; Wang, Fen; Huang, Genping; Li, Jessica; Li, Xingwei
Journal of publication	Chemical science
Year of publication	2025
Journal volume	16
Journal issue	31
Pages of publication	14252 - 14261
a	9.8872 ± 0.0012 Å
b	31.082 ± 0.004 Å
c	11.0103 ± 0.0014 Å
α	90°
β	108.905 ± 0.004°
γ	90°
Cell volume	3201.1 ± 0.7 Å³
Cell temperature	243 K
Ambient diffraction temperature	243 K
Number of distinct elements	5
Space group number	4
Hermann-Mauguin space group symbol	P 1 21 1
Hall space group symbol	P 2yb
Residual factor for all reflections	0.0906
Residual factor for significantly intense reflections	0.0895
Weighted residual factors for significantly intense reflections	0.2533
Weighted residual factors for all reflections included in the refinement	0.2551
Goodness-of-fit parameter for all reflections included in the refinement	0.995
Diffraction radiation wavelength	1.54178 Å
Diffraction radiation type	CuKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

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