Information card for entry 1575102

Structure parameters

• Formula: C92 H94 N6 Na4 O33 S3 Si2
• Calculated formula: C84 H74.0004 N6 Na3.9999 O31 S3 Si2
• Title of publication: Construction of helicates based on six-coordinated silicon centres.
• Authors of publication: Guan, Yu-Tao; Ji, Heng; Yang, Ju; Yu, Sai-Sai; Liu, Ming
• Journal of publication: Chemical science
• Year of publication: 2025
• Journal volume: 16
• Journal issue: 32
• Pages of publication: 14448 - 14454
• a: 15.2692 ± 0.0002 Å
• b: 15.2692 ± 0.0002 Å
• c: 28.4569 ± 0.0007 Å
• α: 90°
• β: 90°
• γ: 120°
• Cell volume: 5745.8 ± 0.18 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 7
• Space group number: 159
• Hermann-Mauguin space group symbol: P 3 1 c
• Hall space group symbol: P 3 -2c
• Residual factor for all reflections: 0.077
• Residual factor for significantly intense reflections: 0.0722
• Weighted residual factors for significantly intense reflections: 0.2028
• Weighted residual factors for all reflections included in the refinement: 0.2094
• Goodness-of-fit parameter for all reflections included in the refinement: 1.037
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 1.54178 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No