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Information card for entry 1575491
Preview
| Coordinates | 1575491.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C29 H42 Al Cl4 P2 |
|---|---|
| Calculated formula | C29 H42 Al Cl4 P2 |
| Title of publication | A facile route to <i>cis</i>-olefin-linked phosphino-phosphonium salts of the form: [Ph<sub>2</sub>PC(R)C(H)P(R')<sub>2</sub>H][AlCl<sub>4</sub>]. |
| Authors of publication | Al-Zuhaika, Nahil; Severin, Simon; Schmuckler, Madeleine D.; Lough, Alan J.; Stephan, Douglas W. |
| Journal of publication | Chemical communications (Cambridge, England) |
| Year of publication | 2025 |
| Journal volume | 61 |
| Journal issue | 77 |
| Pages of publication | 14967 - 14970 |
| a | 10.79 ± 0.002 Å |
| b | 12.56 ± 0.002 Å |
| c | 13.068 ± 0.002 Å |
| α | 92.792 ± 0.011° |
| β | 94.984 ± 0.012° |
| γ | 108.606 ± 0.011° |
| Cell volume | 1666.6 ± 0.5 Å3 |
| Cell temperature | 149.99 K |
| Ambient diffraction temperature | 149.99 K |
| Number of distinct elements | 5 |
| Space group number | 2 |
| Hermann-Mauguin space group symbol | P -1 |
| Hall space group symbol | -P 1 |
| Residual factor for all reflections | 0.1489 |
| Residual factor for significantly intense reflections | 0.1012 |
| Weighted residual factors for significantly intense reflections | 0.2621 |
| Weighted residual factors for all reflections included in the refinement | 0.301 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.0781 |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | No |
| Has Fobs | No |
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The link is: https://www.crystallography.net/1575491.html
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