Information card for entry 1575789

Structure parameters

• Formula: C62 H86 Ge2 N2 P2 Si2
• Calculated formula: C62 H86 Ge2 N2 P2 Si2
• Title of publication: The path to an open-shell metallo-germylene: direct ligation, or reduction and metathesis?
• Authors of publication: Schulz, Annika; Heinz, Myron; Holthausen, Max C.; Hadlington, Terrance J.
• Journal of publication: Chemical science
• Year of publication: 2025
• Journal volume: 16
• Journal issue: 43
• Pages of publication: 20265 - 20274
• a: 13.86 ± 0.003 Å
• b: 10.42 ± 0.002 Å
• c: 20.49 ± 0.004 Å
• α: 90°
• β: 93.4 ± 0.03°
• γ: 90°
• Cell volume: 2954 ± 1 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.1025
• Residual factor for significantly intense reflections: 0.0576
• Weighted residual factors for significantly intense reflections: 0.13
• Weighted residual factors for all reflections included in the refinement: 0.1547
• Goodness-of-fit parameter for all reflections included in the refinement: 0.981
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No