Information card for entry 1575929

Structure parameters

• Formula: C48 H108 O16 Pr Si4
• Calculated formula: C48 H108 O16 Pr Si4
• Title of publication: Accessing homoleptic neutral and anionic five-coordinate Pr(iv) siloxide complexes.
• Authors of publication: Pandey, Pragati; Keener, Megan; Rajeshkumar, Thayalan; Scopelliti, Rosario; Sienkiewicz, Andrzej; Zivkovic, Ivica; Maron, Laurent; Mazzanti, Marinella
• Journal of publication: Chemical science
• Year of publication: 2025
• Journal volume: 16
• Journal issue: 44
• Pages of publication: 21056 - 21067
• a: 24.1029 ± 0.0003 Å
• b: 13.5279 ± 0.0002 Å
• c: 40.7549 ± 0.0006 Å
• α: 90°
• β: 96.2414 ± 0.0015°
• γ: 90°
• Cell volume: 13209.8 ± 0.3 ų
• Cell temperature: 139.99 ± 0.1 K
• Ambient diffraction temperature: 139.99 ± 0.1 K
• Number of distinct elements: 5
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.077
• Residual factor for significantly intense reflections: 0.0684
• Weighted residual factors for significantly intense reflections: 0.141
• Weighted residual factors for all reflections included in the refinement: 0.1454
• Goodness-of-fit parameter for all reflections included in the refinement: 1.183
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 1.54184 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No