Information card for entry 1575981

Structure parameters

• Formula: C28 H27 N O3 Si
• Calculated formula: C28 H27 N O3 Si
• Title of publication: Catalytic asymmetric synthesis of indole-based atropisomers bearing silicon-stereogenic centers.
• Authors of publication: Liu, Si-Yi; Zhu, Zi-Qi; Chen, Fei-Xiao; Feng, Ni-Na; Ni, Shao-Fei; Shi, Feng
• Journal of publication: Chemical science
• Year of publication: 2025
• Journal volume: 16
• Journal issue: 45
• Pages of publication: 21394 - 21403
• a: 11.254 ± 0.003 Å
• b: 8.328 ± 0.002 Å
• c: 13.391 ± 0.004 Å
• α: 90°
• β: 91.61 ± 0.011°
• γ: 90°
• Cell volume: 1254.6 ± 0.6 ų
• Cell temperature: 170 K
• Ambient diffraction temperature: 170 K
• Number of distinct elements: 5
• Space group number: 4
• Hermann-Mauguin space group symbol: P 1 21 1
• Hall space group symbol: P 2yb
• Residual factor for all reflections: 0.1658
• Residual factor for significantly intense reflections: 0.0842
• Weighted residual factors for significantly intense reflections: 0.2107
• Weighted residual factors for all reflections included in the refinement: 0.2601
• Goodness-of-fit parameter for all reflections included in the refinement: 1.001
• Diffraction radiation wavelength: 1.34139 Å
• Diffraction radiation type: GaKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No