Information card for entry 1576101

Structure parameters

• Formula: C91 H123 Cl3 O4 Si4
• Calculated formula: C90 H122 O4 Si4
• Title of publication: One-pot synthesis of sequence-controlled macromonomers <i>via</i> living anionic addition reaction and subsequent acyclic diene metathesis polymerization.
• Authors of publication: Nishijima, Tomohiko; Takahata, Kazuki; Goseki, Raita; Homma, Chihiro; Kuwata, Shigeki; Ishizone, Takashi
• Journal of publication: Chemical science
• Year of publication: 2025
• Journal volume: 16
• Journal issue: 46
• Pages of publication: 21791 - 21796
• a: 14.995 ± 0.003 Å
• b: 15.093 ± 0.003 Å
• c: 19.626 ± 0.003 Å
• α: 78.515 ± 0.005°
• β: 89.878 ± 0.006°
• γ: 85.166 ± 0.005°
• Cell volume: 4336.8 ± 1.4 ų
• Cell temperature: 93 K
• Ambient diffraction temperature: 93 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1579
• Residual factor for significantly intense reflections: 0.1202
• Weighted residual factors for significantly intense reflections: 0.3337
• Weighted residual factors for all reflections included in the refinement: 0.3741
• Goodness-of-fit parameter for all reflections included in the refinement: 1.092
• Diffraction radiation wavelength: 0.71075 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No