Information card for entry 1576234

Structure parameters

• Formula: C43.7 H6.2 Ag B2 Cl6.2 F30 N Ni0.9 O3.6
• Calculated formula: C42.7 H4.2 Ag B2 Cl4.2 F30 N Ni0.9 O3.6
• Title of publication: A facile route to ‘naked’ Ag+ ions enabling the coordination of the weak Lewis base Ni(CO)4
• Authors of publication: Berg, Willi Ragnar; Moshtaha, Amina Leoni; Sievers, Robin; Reimann, Marc; Streit, Tim-Niclas; Rupf, Susanne M.; Kaupp, Martin; Malischewski, Moritz
• Journal of publication: Chemical Science
• Year of publication: 2025
• a: 13.288 ± 0.0005 Å
• b: 28.0807 ± 0.001 Å
• c: 13.7219 ± 0.0004 Å
• α: 90°
• β: 91.614 ± 0.001°
• γ: 90°
• Cell volume: 5118.1 ± 0.3 ų
• Cell temperature: 100 K
• Ambient diffraction temperature: 100 K
• Number of distinct elements: 9
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0595
• Residual factor for significantly intense reflections: 0.0444
• Weighted residual factors for significantly intense reflections: 0.1064
• Weighted residual factors for all reflections included in the refinement: 0.1188
• Goodness-of-fit parameter for all reflections included in the refinement: 1.059
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No