Information card for entry 1576860

Structure parameters

• Formula: C20 H24 N2 Ni O2
• Calculated formula: C20 H24 N2 Ni O2
• Title of publication: Ring-opening decarbonylative C(sp3)–C(sp3) cross-electrophile coupling of cyclic imides with unactivated alkyl chlorides
• Authors of publication: Lentelink, Niklas J.; Pânzar, Peter M. F.; Rowlinson, Nathalie A. V.; Morandi, Bill
• Journal of publication: Chemical Science
• Year of publication: 2026
• a: 22.0314 ± 0.0003 Å
• b: 20.8413 ± 0.0003 Å
• c: 8.4416 ± 0.0001 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 3876.07 ± 0.09 ų
• Cell temperature: 100 ± 0.1 K
• Ambient diffraction temperature: 100 ± 0.1 K
• Number of distinct elements: 5
• Space group number: 43
• Hermann-Mauguin space group symbol: F d d 2
• Hall space group symbol: F 2 -2d
• Residual factor for all reflections: 0.0358
• Residual factor for significantly intense reflections: 0.0337
• Weighted residual factors for significantly intense reflections: 0.0889
• Weighted residual factors for all reflections included in the refinement: 0.0906
• Goodness-of-fit parameter for all reflections included in the refinement: 1.109
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 1.54184 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No