Information card for entry 1576983
| Formula |
C12 H15 N O3 Si |
| Calculated formula |
C12 H15 N O3 Si |
| Title of publication |
Nickel-catalyzed hydroxymethylation with α-silicon <i>N</i>-methoxyphthalimides <i>via</i> radical Brook rearrangement. |
| Authors of publication |
Liu, Xiao-Bo; Bilal, Muhammad; Zuo, Jiaying; Yu, Ya-Xin; Wu, Yu-Juan; Shen, Boming; Shen, Peng-Hui; Xu, Hua-Jian; Liang, Yu-Feng |
| Journal of publication |
Chemical science |
| Year of publication |
2026 |
| Journal volume |
17 |
| Journal issue |
19 |
| Pages of publication |
9653 - 9662 |
| a |
6.0357 ± 0.0015 Å |
| b |
19.028 ± 0.005 Å |
| c |
11.731 ± 0.003 Å |
| α |
90° |
| β |
92.745 ± 0.012° |
| γ |
90° |
| Cell volume |
1345.7 ± 0.6 Å3 |
| Cell temperature |
298 K |
| Ambient diffraction temperature |
298 K |
| Number of distinct elements |
5 |
| Space group number |
14 |
| Hermann-Mauguin space group symbol |
P 1 21/c 1 |
| Hall space group symbol |
-P 2ybc |
| Residual factor for all reflections |
0.0648 |
| Residual factor for significantly intense reflections |
0.0499 |
| Weighted residual factors for significantly intense reflections |
0.1396 |
| Weighted residual factors for all reflections included in the refinement |
0.1526 |
| Goodness-of-fit parameter for all reflections included in the refinement |
1.083 |
| Diffraction radiation wavelength |
1.54178 Å |
| Diffraction radiation type |
CuKα |
| Has coordinates |
Yes |
| Has disorder |
No |
| Has Fobs |
No |
For the version history of this entry, please navigate to main COD server.
The link is:
https://www.crystallography.net/1576983.html
