Information card for entry 1577336

Structure parameters

• Formula: C97 H134 B Cl Ge2 K2 O
• Calculated formula: C97 H134 B Cl Ge2 K2 O
• Title of publication: Three reversibly interconvertible redox states of boradigermaallyl: syntheses of radical allyl anion and allyl dianion.
• Authors of publication: Miehe, Stefan F.; Eichele, Klaus; Schubert, Hartmut; Bettinger, Holger F.; Sindlinger, Christian P.; Wesemann, Lars
• Journal of publication: Chemical science
• Year of publication: 2026
• Journal volume: 17
• Journal issue: 17
• Pages of publication: 8622 - 8629
• a: 15.3084 ± 0.0004 Å
• b: 15.6697 ± 0.0004 Å
• c: 20.0999 ± 0.0005 Å
• α: 80.717 ± 0.001°
• β: 86.317 ± 0.001°
• γ: 72.398 ± 0.001°
• Cell volume: 4535 ± 0.2 ų
• Cell temperature: 120 ± 2 K
• Ambient diffraction temperature: 120 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0529
• Residual factor for significantly intense reflections: 0.0392
• Weighted residual factors for significantly intense reflections: 0.1017
• Weighted residual factors for all reflections included in the refinement: 0.1091
• Goodness-of-fit parameter for all reflections included in the refinement: 1.026
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No