Information card for entry 1577338

Structure parameters

• Formula: C95 H130 B Cl Ge2 K O3
• Calculated formula: C95 H130 B Cl Ge2 K O3
• Title of publication: Three reversibly interconvertible redox states of boradigermaallyl: syntheses of radical allyl anion and allyl dianion.
• Authors of publication: Miehe, Stefan F.; Eichele, Klaus; Schubert, Hartmut; Bettinger, Holger F.; Sindlinger, Christian P.; Wesemann, Lars
• Journal of publication: Chemical science
• Year of publication: 2026
• Journal volume: 17
• Journal issue: 17
• Pages of publication: 8622 - 8629
• a: 13.9575 ± 0.0003 Å
• b: 24.6291 ± 0.0004 Å
• c: 25.533 ± 0.0005 Å
• α: 90°
• β: 98.924 ± 0.001°
• γ: 90°
• Cell volume: 8671 ± 0.3 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0744
• Residual factor for significantly intense reflections: 0.0563
• Weighted residual factors for significantly intense reflections: 0.1363
• Weighted residual factors for all reflections included in the refinement: 0.146
• Goodness-of-fit parameter for all reflections included in the refinement: 1.063
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No