Information card for entry 2003955

Structure parameters

• Formula: C26 H36 Cl2 N Os P3
• Calculated formula: C26 H36 Cl2 N Os P3
• Title of publication: (Acetonitrile)-<i>trans</i>-dichloro-<i>mer</i>-tris[(dimethyl)phenylphosphine]osmium(III); the Kinetically Controlled Electrogenerated Isomer
• Authors of publication: Yeomans, B. D.; Heath, G. A.; Hockless, D. C. R.
• Journal of publication: Acta Crystallographica Section C
• Year of publication: 1995
• Journal volume: 51
• Journal issue: 9
• Pages of publication: 1807 - 1809
• a: 9.132 ± 0.002 Å
• b: 12.248 ± 0.002 Å
• c: 13.622 ± 0.003 Å
• α: 95.72 ± 0.02°
• β: 105.6 ± 0.02°
• γ: 89.91 ± 0.02°
• Cell volume: 1459.7 ± 0.5 ų
• Cell temperature: 295 K
• Ambient diffraction temperature: 295 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0609
• Residual factor for significantly intense reflections: 0.044
• Weighted residual factors for all reflections: 0.0622
• Weighted residual factors for significantly intense reflections: 0.061
• Goodness-of-fit parameter for significantly intense reflections: 2.59
• Diffraction radiation wavelength: 0.7107 Å
• Diffraction radiation type: MoKalpha
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No