Information card for entry 2003961

Structure parameters

• Formula: C14 H32 Cl2 N4 Ni O8
• Calculated formula: C14 H32 Cl2 N4 Ni O8
• Title of publication: [(5<i>SR</i>,7<i>RS</i>,12<i>RS</i>,14<i>RS</i>)-5,7,12,14-Tetramethyl-1,4,8,11-tetraazacyclotetradecane]nickel(II) Diperchlorate
• Authors of publication: Tahirov, T. H.; Lu, T.-H.; Liu, G.-S.; Chi, T.-Y.; Chung, C.-S.
• Journal of publication: Acta Crystallographica Section C
• Year of publication: 1995
• Journal volume: 51
• Journal issue: 10
• Pages of publication: 2018 - 2020
• a: 15.665 ± 0.001 Å
• b: 16.352 ± 0.003 Å
• c: 17.252 ± 0.001 Å
• α: 90°
• β: 95.725 ± 0.007°
• γ: 90°
• Cell volume: 4397.1 ± 0.9 ų
• Cell temperature: 298 ± 3 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/a 1
• Hall space group symbol: -P 2yab
• Residual factor for significantly intense reflections: 0.048
• Weighted residual factors for significantly intense reflections: 0.058
• Goodness-of-fit parameter for significantly intense reflections: 1.38
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No