Information card for entry 2004096

Structure parameters

• Chemical name: 3,3,7,7,10,10-Hexaphenyl-2,4,6,8,9,11-hexaoxa-1,5-diarsa-3,7,10-trisila- bicyclo[3,3,3]undecane
• Formula: C36 H30 As2 O6 Si3
• Calculated formula: C36 H30 As2 O6 Si3
• Title of publication: An As~2~Si~3~O~6~ Cage Compound, 3,3,7,7,10,10-Hexaphenyl-2,4,6,8,9,11-hexaoxa-1,5-diarsa-3,7,10-trisilabicyclo[3.3.3]undecane
• Authors of publication: Ferguson, G.; O'Leary, B.; Spalding, T. R.
• Journal of publication: Acta Crystallographica Section C
• Year of publication: 1995
• Journal volume: 51
• Journal issue: 11
• Pages of publication: 2312 - 2315
• a: 8.2444 ± 0.0015 Å
• b: 10.7401 ± 0.0013 Å
• c: 20.049 ± 0.003 Å
• α: 90°
• β: 95.057 ± 0.014°
• γ: 90°
• Cell volume: 1768.3 ± 0.5 ų
• Cell temperature: 294 ± 1 K
• Ambient diffraction temperature: 294 ± 1 K
• Number of distinct elements: 5
• Space group number: 4
• Hermann-Mauguin space group symbol: P 1 21 1
• Hall space group symbol: P 2yb
• Residual factor for all reflections: 0.043
• Residual factor for significantly intense reflections: 0.029
• Weighted residual factors for all reflections: 0.04
• Weighted residual factors for significantly intense reflections: 0.038
• Goodness-of-fit parameter for significantly intense reflections: 1.06
• Diffraction radiation wavelength: 0.7107 Å
• Diffraction radiation type: MolybdenumKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No