Information card for entry 2004131

Structure parameters

• Chemical name: (1S,8S,8aS)-(+)-1-(t-Butyldimethylsilyloxy)-8-hydroxy-5-indolizidinone
• Formula: C14 H27 N O3 Si
• Calculated formula: C14 H27 N O3 Si
• Title of publication: (1<i>S</i>,8<i>S</i>,8a<i>S</i>)-(+)-1-(<i>tert</i>-Butyldimethylsilyloxy)-8-hydroxy-1,2,3,5,6,7,8,8a-octahydro-5-indolizinone
• Authors of publication: Hua, D. H.; Lagneau, N.; Park, J.-G.; Good, L. A.; Robinson, P. D.
• Journal of publication: Acta Crystallographica Section C
• Year of publication: 1995
• Journal volume: 51
• Journal issue: 11
• Pages of publication: 2301 - 2304
• a: 7.203 ± 0.003 Å
• b: 34.626 ± 0.005 Å
• c: 7.048 ± 0.001 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 1757.8 ± 0.8 ų
• Cell temperature: 296 K
• Ambient diffraction temperature: 296 K
• Number of distinct elements: 5
• Space group number: 19
• Hermann-Mauguin space group symbol: P 21 21 21
• Hall space group symbol: P 2ac 2ab
• Residual factor for significantly intense reflections: 0.054
• Weighted residual factors for significantly intense reflections: 0.059
• Goodness-of-fit parameter for significantly intense reflections: 1.8
• Diffraction radiation wavelength: 0.71069 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No