Information card for entry 2006236

Structure parameters

• Chemical name: (3S,4R,5R)-5,6-diacetoxy-4-(t-butyldiphenylsilyloxy)-3-hydroxy -4-methylhex-1-en
• Formula: C27 H36 O6 Si
• Calculated formula: C27 H36 O6 Si
• Title of publication: (2<i>R</i>,3<i>R</i>,4<i>S</i>)-3-(<i>tert</i>-Butyldiphenylsiloxy)-4-hydroxy-3-methylhex-5-ene-1,2-diyl Diacetate
• Authors of publication: Lewinski, Krzysztof
• Journal of publication: Acta Crystallographica Section C
• Year of publication: 1997
• Journal volume: 53
• Journal issue: 6
• Pages of publication: 753 - 755
• a: 10.838 ± 0.001 Å
• b: 9.347 ± 0.001 Å
• c: 13.456 ± 0.001 Å
• α: 90°
• β: 92.3 ± 0.01°
• γ: 90°
• Cell volume: 1362 ± 0.2 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 4
• Space group number: 4
• Hermann-Mauguin space group symbol: P 1 21 1
• Hall space group symbol: P 2yb
• Residual factor for all reflections: 0.0345
• Residual factor for significantly intense reflections: 0.0317
• Weighted residual factors for all reflections: 0.0869
• Weighted residual factors for significantly intense reflections: 0.0856
• Goodness-of-fit parameter for all reflections: 1.021
• Goodness-of-fit parameter for significantly intense reflections: 1.037
• Diffraction radiation wavelength: 0.71069 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No