Information card for entry 2007109

Structure parameters

• Formula: C30 H94 Mo12 N15 O47 P5 Si
• Calculated formula: C30 H92 Mo12 N15 O46.5 P5 Si
• Title of publication: A Dihydrate Complex of Molybdosilicic Acid and Hexamethylphosphoramide, [{(CH~3~)~2~N}~3~PO]~5~[H~4~SiMo~12~O~40~].2H~2~O
• Authors of publication: Fun, Hoong-Kun; Chinnakali, Kandasamy; Yip, Boon-Chuan; Niu, Jing-Yang; Wang, Jing-Ping; You, Xiao-Zeng
• Journal of publication: Acta Crystallographica Section C
• Year of publication: 1998
• Journal volume: 54
• Journal issue: 3
• Pages of publication: 327 - 329
• a: 13.849 ± 0.001 Å
• b: 13.94 ± 0.001 Å
• c: 22.024 ± 0.002 Å
• α: 95.77 ± 0.01°
• β: 99.45 ± 0.01°
• γ: 91.51 ± 0.01°
• Cell volume: 4168.9 ± 0.6 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.065
• Residual factor for significantly intense reflections: 0.044
• Weighted residual factors for all reflections: 0.125
• Weighted residual factors for significantly intense reflections: 0.116
• Goodness-of-fit parameter for all reflections: 0.961
• Goodness-of-fit parameter for significantly intense reflections: 1.07
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No