Information card for entry 2007575

Structure parameters

• Chemical name: (1,4-bis(diphenylphosphino-k,P,P')butane)(N,N'-diethyldithiocarbamato)- nickel(II) perchlorate.
• Formula: C33 H38 Cl N Ni O4 P2 S2
• Calculated formula: C33 H38 Cl N Ni O4 P2 S2
• Title of publication: [1,4-Bis(diphenylphosphino)butane-<i>P</i>,<i>P</i>'](<i>N</i>,<i>N</i>'-diethyldithiocarbamato-<i>S</i>,<i>S</i>')nickel(II) Perchlorate
• Authors of publication: Ramalingam,Kuppukkannu; Shawkataly, Omar bin; Fun, Hoong-Kun; Ibrahim,Abdul Razak
• Journal of publication: Acta Crystallographica Section C
• Year of publication: 1998
• Journal volume: 54
• Journal issue: 9
• Pages of publication: 1223 - 1225
• a: 18.951 ± 0.001 Å
• b: 9.104 ± 0.001 Å
• c: 20.842 ± 0.002 Å
• α: 90°
• β: 100.01 ± 0.01°
• γ: 90°
• Cell volume: 3541.1 ± 0.6 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 8
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0713
• Residual factor for significantly intense reflections: 0.0441
• Weighted residual factors for all reflections: 0.1314
• Weighted residual factors for significantly intense reflections: 0.1193
• Goodness-of-fit parameter for all reflections: 0.945
• Goodness-of-fit parameter for significantly intense reflections: 1.076
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No