Information card for entry 2008489

Structure parameters

• Formula: C15 H16 N4 Ni O3
• Calculated formula: C14.5 H16 N4 Ni0.5 O2.5
• Title of publication: [1,3-Bis(pyridine-2-carboxamido)propane]palladium(II) monohydrate and its nickel(II) analogue
• Authors of publication: Tamura, Masana; Kajikawa, Yuji; Azuma, Nagao; Tani, Hiroyuki; Tajima, Kunihiko; Kanaori, Kenji; Makino, Keisuke; Takayama, Toshio
• Journal of publication: Acta Crystallographica Section C
• Year of publication: 1999
• Journal volume: 55
• Journal issue: 5
• Pages of publication: 719 - 722
• a: 7.183 ± 0.002 Å
• b: 9.307 ± 0.003 Å
• c: 11.326 ± 0.003 Å
• α: 90°
• β: 105.73 ± 0.02°
• γ: 90°
• Cell volume: 728.8 ± 0.4 ų
• Cell temperature: 298.2 K
• Ambient diffraction temperature: 298.2 K
• Number of distinct elements: 5
• Space group number: 13
• Hermann-Mauguin space group symbol: P 1 2/n 1
• Hall space group symbol: -P 2yac
• Residual factor for significantly intense reflections: 0.043
• Weighted residual factors for all reflections included in the refinement: 0.045
• Goodness-of-fit parameter for all reflections included in the refinement: 1.674
• Diffraction radiation wavelength: 0.7107 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No