Information card for entry 2008676

Structure parameters

• Common name: Ni(t-salpd)
• Formula: C18 H18 N2 Ni O0.5 S2
• Calculated formula: C18 H18 N2 Ni O0.5 S2
• Title of publication: A nickel complex with a tetradentate N~2~S~2~ Schiff base ligand
• Authors of publication: Gomes, Ligia; Pereira, Eulalia; de Castro, Baltazar
• Journal of publication: Acta Crystallographica Section C
• Year of publication: 1999
• Journal volume: 55
• Journal issue: 7
• Pages of publication: 1061 - 1063
• a: 17 ± 0.002 Å
• b: 14.369 ± 0.002 Å
• c: 13.485 ± 0.002 Å
• α: 90°
• β: 91.32 ± 0.01°
• γ: 90°
• Cell volume: 3293.1 ± 0.8 ų
• Cell temperature: 298 ± 2 K
• Ambient diffraction temperature: 298 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.067
• Residual factor for significantly intense reflections: 0.043
• Weighted residual factors for all reflections: 0.121
• Weighted residual factors for significantly intense reflections: 0.099
• Goodness-of-fit parameter for all reflections: 1.215
• Goodness-of-fit parameter for significantly intense reflections: 1.217
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No