Information card for entry 2009163

Structure parameters

• Chemical name: Tris[3,6-bis(2'-pyridyl)pyridazine-N^1^,N^6^]nickel(II) diperchlorate 0.11-hydrate
• Formula: C42 H30.22 Cl2 N12 Ni O8.11
• Calculated formula: C42 H30.226 Cl2 N12 Ni O8.113
• Title of publication: Tris[3,6-bis(2-pyridyl)pyridazine-<i>N</i>^1^,<i>N</i>^6^]nickel(II) diperchlorate 0.11-hydrate
• Authors of publication: Jau-Shuenn Wang; Chou-Fu Sheu; Jung-Si Lee
• Journal of publication: Acta Crystallographica Section C
• Year of publication: 1999
• Journal volume: 55
• Journal issue: 11
• Pages of publication: 1806 - 1809
• a: 16.249 ± 0.002 Å
• b: 16.3338 ± 0.0012 Å
• c: 17.414 ± 0.003 Å
• α: 81.362 ± 0.01°
• β: 87.18 ± 0.012°
• γ: 67.335 ± 0.009°
• Cell volume: 4216.3 ± 1 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.096
• Residual factor for significantly intense reflections: 0.057
• Weighted residual factors for all reflections: 0.168
• Weighted residual factors for significantly intense reflections: 0.139
• Goodness-of-fit parameter for all reflections: 1.046
• Goodness-of-fit parameter for significantly intense reflections: 1.081
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No