Information card for entry 2009654

Structure parameters

• Common name: Tetraphenylphosphophonium hexachlorodioxo-μ-dichlorophospato-μ-nitrido- ditungstide
• Formula: C48 H40 Cl8 N O4 P3 W2
• Calculated formula: C48 H40 Cl8 N O4 P3 W2
• Title of publication: [Me~3~PhN]~2~[WCl~6~] und [PPh~4~]~2~[W~2~Cl~6~O~2~(μ-N)(μ-Cl~2~PO~2~)], ein μ-<i>N</i>-Nitridowolframat mit Dichlorophosphatbrücke
• Authors of publication: Müller, Ulrich; Sens, Irina; Wollert, René; Dehnicke, Kurt
• Journal of publication: Acta Crystallographica Section C
• Year of publication: 1994
• Journal volume: 50
• Journal issue: 4
• Pages of publication: 493 - 496
• a: 27.369 ± 0.007 Å
• b: 11.349 ± 0.002 Å
• c: 18.451 ± 0.004 Å
• α: 90°
• β: 115.36 ± 0.04°
• γ: 90°
• Cell volume: 5179 ± 3 ų
• Cell temperature: 293 K
• Ambient diffraction temperature: 293 K
• Number of distinct elements: 7
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.061
• Residual factor for significantly intense reflections: 0.041
• Weighted residual factors for significantly intense reflections: 0.03
• Goodness-of-fit parameter for significantly intense reflections: 1.5
• Diffraction radiation wavelength: 0.7107 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No