Information card for entry 2011107

Structure parameters

• Chemical name: μ-oxo-bis{oxo{2,2'-[propane-1,3-diylbis(nitrilomethylidyne)]diphenolato} rhenium(V)} dichloromethane solvate (1:2)
• Formula: C36 H36 Cl4 N4 O7 Re2
• Calculated formula: C36 H36 Cl4 N4 O7 Re2
• Title of publication: Polymorphs and pseudo-polymorphs of μ-oxo-bis{[<i>N</i>,<i>N</i>'-bis(salicylidene)propane-1,3-diamine]oxorhenium(V)}
• Authors of publication: Kooijman, Huub; Bommel, Kjeld J. C. van; Verboom, Willem; Reinhoudt, David N.; Kroon, Jan; Spek, Anthony L.
• Journal of publication: Acta Crystallographica Section C
• Year of publication: 2000
• Journal volume: 56
• Journal issue: 7
• Pages of publication: 749 - 757
• a: 8.9642 ± 0.0016 Å
• b: 10.053 ± 0.003 Å
• c: 10.669 ± 0.003 Å
• α: 91.23 ± 0.02°
• β: 91.685 ± 0.018°
• γ: 97.913 ± 0.017°
• Cell volume: 951.6 ± 0.4 ų
• Cell temperature: 150 K
• Ambient diffraction temperature: 150 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.051
• Residual factor for significantly intense reflections: 0.049
• Weighted residual factors for all reflections included in the refinement: 0.137
• Goodness-of-fit parameter for all reflections included in the refinement: 1.06
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: Yes