Information card for entry 2011166

Structure parameters

• Chemical name: tetrakis(ethylenediammonium) tetra-μ-hydrogenphosphato-di-μ-hydroxo- tetra-μ-phosphato-bis(aquacobalt)hexakis(oxovanadium) trihydrate
• Formula: C8 H56 Co N8 O45 P8 V6
• Calculated formula: C8 H40 Co N8 O45 P8 V6
• Title of publication: A hydrated ethylenediammonium salt of a new polymeric polyoxoanion: (H~2~en)~4~[Co(H~2~O)~2~(OH)~2~(VO)~6~(HPO~4~)~4~(PO~4~)~4~]·3H~2~O
• Authors of publication: Luan, Guo-You; Wang, En-Bo; You, Wan-Sheng; Xu, Lin; He, Qin-Lin
• Journal of publication: Acta Crystallographica Section C
• Year of publication: 2000
• Journal volume: 56
• Journal issue: 7
• Pages of publication: e284 - e285
• a: 20.709 ± 0.004 Å
• b: 9.968 ± 0.002 Å
• c: 23.66 ± 0.005 Å
• α: 90°
• β: 101.04 ± 0.03°
• γ: 90°
• Cell volume: 4793.7 ± 1.7 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 7
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.054
• Residual factor for significantly intense reflections: 0.046
• Weighted residual factors for all reflections: 0.137
• Weighted residual factors for significantly intense reflections: 0.134
• Goodness-of-fit parameter for all reflections: 1.123
• Goodness-of-fit parameter for significantly intense reflections: 1.211
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No