Information card for entry 2011176

Structure parameters

• Chemical name: Bis[methylenebis(diphenylphosphine)-P,P']nickel(II) diperchlorate
• Formula: C50 H44 Cl2 Ni O8 P4
• Calculated formula: C50 H44 Cl2 Ni O8 P4
• SMILES: Cl(=O)(=O)(=O)[O-].[Ni]12([P](C[P]1(c1ccccc1)c1ccccc1)(c1ccccc1)c1ccccc1)[P](C[P]2(c1ccccc1)c1ccccc1)(c1ccccc1)c1ccccc1.Cl(=O)(=O)(=O)[O-]
• Title of publication: Bis[methylenebis(diphenylphosphine)-<i>P</i>,<i>P</i>']nickel(II) diperchlorate
• Authors of publication: Li, Yi-Zhi; Liu, Jia-Cheng; Wang, Zhi-Ping; Li, Qin-Xi; Sun, Gang-Chun; Wang, Liu-Fang; Xia, Chun-Gu
• Journal of publication: Acta Crystallographica Section C
• Year of publication: 2000
• Journal volume: 56
• Journal issue: 7
• Pages of publication: e286 - e287
• a: 11.226 ± 0.002 Å
• b: 17.836 ± 0.002 Å
• c: 12.932 ± 0.002 Å
• α: 90°
• β: 111.32 ± 0.01°
• γ: 90°
• Cell volume: 2412.1 ± 0.7 ų
• Cell temperature: 296 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for significantly intense reflections: 0.033
• Weighted residual factors for all reflections included in the refinement: 0.044
• Goodness-of-fit parameter for all reflections included in the refinement: 1.22
• Diffraction radiation wavelength: 0.71069 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: Yes