Information card for entry 2013443

Structure parameters

• Chemical name: Cis-{[1,4-(diphenylphosphine-P,P')butane] [μ-(tetrathiotungstate-S,S')]}Pd(II)0.5N,N'-dimethylformamide 0.5hydrate
• Formula: C29.5 H32.5 N0.5 O P2 Pd S4 W
• Calculated formula: C29.5 H32.5 N0.5 O P2 Pd S4 W
• Title of publication: <i>cis</i>-[1,4-Bis(diphenylphosphino)butane](μ-tetrathiotungstato)palladium(II) <i>N</i>,<i>N</i>'-dimethylformamide hemisolvate hemihydrate
• Authors of publication: Liang, Kai; Li, Yi-Zhi; Zheng, He-Gen; Xin, Xin-Quan
• Journal of publication: Acta Crystallographica Section C
• Year of publication: 2003
• Journal volume: 59
• Journal issue: 8
• Pages of publication: m310 - m312
• a: 9.178 ± 0.001 Å
• b: 19.566 ± 0.002 Å
• c: 19.705 ± 0.002 Å
• α: 90°
• β: 98.44 ± 0.01°
• γ: 90°
• Cell volume: 3500.2 ± 0.6 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 8
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0635
• Residual factor for significantly intense reflections: 0.0377
• Weighted residual factors for significantly intense reflections: 0.1018
• Weighted residual factors for all reflections included in the refinement: 0.1084
• Goodness-of-fit parameter for all reflections included in the refinement: 1.045
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: Yes