Information card for entry 2014303

Structure parameters

• Chemical name: {tert-Butyl[(E)-2-(tert-butylimino)ethyl]amido-k^2^N,N'} [bis(trimethylsilyl)amido-κN]tin(II)
• Formula: C16 H39 N3 Si2 Sn
• Calculated formula: C16 H39 N3 Si2 Sn
• Title of publication: [Bis(trimethylsilyl)amido-κ<i>N</i>]{<i>tert</i>-butyl[(<i>E</i>)-2-(<i>tert</i>-butylimino)ethyl]amido-κ^2^<i>N</i>,<i>N</i>'}tin(II), a key intermediate in the synthesis of 1,3-di-<i>tert</i>-butyl-2,3-dihydro-1<i>H</i>-1,3,2-diazastannole
• Authors of publication: Guzei, Ilia A.; Timokhin, Vitaliy I.; West, Robert
• Journal of publication: Acta Crystallographica Section C
• Year of publication: 2006
• Journal volume: 62
• Journal issue: 3
• Pages of publication: m90 - m92
• a: 9.2875 ± 0.0003 Å
• b: 10.3056 ± 0.0003 Å
• c: 13.3897 ± 0.0004 Å
• α: 81.468 ± 0.001°
• β: 85.416 ± 0.001°
• γ: 64.27 ± 0.001°
• Cell volume: 1141.55 ± 0.06 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0332
• Residual factor for significantly intense reflections: 0.0311
• Weighted residual factors for significantly intense reflections: 0.0784
• Weighted residual factors for all reflections included in the refinement: 0.0798
• Goodness-of-fit parameter for all reflections included in the refinement: 1.091
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: Mo-Kα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: Yes