Information card for entry 2015734

Structure parameters

• Chemical name: Poly[1,4,8,11-tetraazacyclotetradecane(2+) [hepta-μ-sulfido-trisulfidohexaantimony(III)]]
• Formula: C10 H20 N4 S10 Sb6
• Calculated formula: C10 H20 N4 S10 Sb6
• Title of publication: 1,4,8,11-Tetraazacyclotetradecane antimony(III) sulfide
• Authors of publication: Lees, Rachel J. E.; Powell, Anthony V.; Watkin, David J.; Chippindale, Ann M.
• Journal of publication: Acta Crystallographica Section C
• Year of publication: 2007
• Journal volume: 63
• Journal issue: 1
• Pages of publication: m27 - m29
• a: 9.4872 ± 0.0009 Å
• b: 15.4477 ± 0.0014 Å
• c: 10.7567 ± 0.0009 Å
• α: 90°
• β: 105.878 ± 0.004°
• γ: 90°
• Cell volume: 1516.3 ± 0.2 ų
• Cell temperature: 100 K
• Ambient diffraction temperature: 100 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0554
• Residual factor for significantly intense reflections: 0.0492
• Weighted residual factors for all reflections: 0.0382
• Weighted residual factors for significantly intense reflections: 0.0377
• Weighted residual factors for all reflections included in the refinement: 0.0377
• Goodness-of-fit parameter for all reflections included in the refinement: 1.0801
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: Yes