Information card for entry 2016028

Structure parameters

• Chemical name: [1L-3,4-Bis(O-diphenylphosphino)-1,2,5,6-tetra-O-methyl-chiro-inositol- κ^2^P,P'][η^4^-(Z,Z)-cycloocta-1,5-diene]rhodium(I) tetrafluoroborate chloroform solvate
• Formula: C43 H51 B Cl3 F4 O6 P2 Rh
• Calculated formula: C43 H51 B Cl3 F4 O6 P2 Rh
• Title of publication: [1<small>L</small>-3,4-Bis-<i>O</i>-(diphenylphosphino)-1,2,5,6-tetra-<i>O</i>-methyl-<i>chiro</i>-inositol-κ^2^<i>P</i>,<i>P</i>'][η^4^-(<i>Z</i>,<i>Z</i>)-cycloocta-1,5-diene]rhodium(I) tetrafluoridoborate chloroform solvate
• Authors of publication: Gainsford, Graeme J.; Lensink, Cees; Falshaw, Andrew F.
• Journal of publication: Acta Crystallographica Section C
• Year of publication: 2007
• Journal volume: 63
• Journal issue: 7
• Pages of publication: m331 - m334
• a: 9.3231 ± 0.0017 Å
• b: 26.611 ± 0.006 Å
• c: 18.218 ± 0.004 Å
• α: 90°
• β: 91.596 ± 0.007°
• γ: 90°
• Cell volume: 4518.1 ± 1.6 ų
• Cell temperature: 158 ± 2 K
• Ambient diffraction temperature: 158 ± 2 K
• Number of distinct elements: 8
• Space group number: 4
• Hermann-Mauguin space group symbol: P 1 21 1
• Hall space group symbol: P 2yb
• Residual factor for all reflections: 0.0769
• Residual factor for significantly intense reflections: 0.0635
• Weighted residual factors for significantly intense reflections: 0.1419
• Weighted residual factors for all reflections included in the refinement: 0.1502
• Goodness-of-fit parameter for all reflections included in the refinement: 1.07
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: Yes