Information card for entry 2016081

Structure parameters

• Chemical name: (4,7-diphenyl-1,10-phenanthroline-κ^2^N,N')bis(tri-<i>tert</i>- butoxysilanethiolato-κS)lead(II) benzene hemisolvate
• Formula: C51 H73 N2 O6 Pb S2 Si2
• Calculated formula: C51 H73 N2 O6 Pb S2 Si2
• Title of publication: (2,2'-Bipyridine)bis(tri-<i>tert</i>-butoxysilanethiolato-κ<i>S</i>)lead(II) and (4,7-diphenyl-1,10-phenanthroline-κ^2^<i>N</i>,<i>N</i>')bis(tri-<i>tert</i>-butoxysilanethiolato-κ<i>S</i>)lead(II) benzene hemisolvate
• Authors of publication: Chojnacki, Jaroslaw; Kloskowska, Magdalena; Janowska, Urszula; Wojnowski, Wieslaw
• Journal of publication: Acta Crystallographica Section C
• Year of publication: 2007
• Journal volume: 63
• Journal issue: 8
• Pages of publication: m349 - m351
• a: 10.204 ± 0.002 Å
• b: 13.359 ± 0.003 Å
• c: 21.109 ± 0.004 Å
• α: 84.57 ± 0.03°
• β: 83.05 ± 0.03°
• γ: 85.29 ± 0.03°
• Cell volume: 2836.2 ± 1 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0781
• Residual factor for significantly intense reflections: 0.0372
• Weighted residual factors for significantly intense reflections: 0.0983
• Weighted residual factors for all reflections included in the refinement: 0.118
• Goodness-of-fit parameter for all reflections included in the refinement: 1.002
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: Yes