Information card for entry 2016687

Structure parameters

• Chemical name: (2,2'-diazenediyldiphenolato-κ^3^<i>O</i>,<i>N</i>,<i>O</i>')dimethylsilicon
• Formula: C14 H14 N2 O2 Si
• Calculated formula: C14 H14 N2 O2 Si
• Title of publication: Dynamic disorder in a pentacoordinate silicon complex with 2,2'-diazenediyldiphenol
• Authors of publication: Böhme, Uwe; Jähnigen, Sandra
• Journal of publication: Acta Crystallographica Section C
• Year of publication: 2008
• Journal volume: 64
• Journal issue: 7
• Pages of publication: o364 - o366
• a: 10.0248 ± 0.001 Å
• b: 7.8879 ± 0.0008 Å
• c: 32.162 ± 0.003 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 2543.2 ± 0.4 ų
• Cell temperature: 93 ± 2 K
• Ambient diffraction temperature: 93 ± 2 K
• Number of distinct elements: 5
• Space group number: 61
• Hermann-Mauguin space group symbol: P b c a
• Hall space group symbol: -P 2ac 2ab
• Residual factor for all reflections: 0.0368
• Residual factor for significantly intense reflections: 0.0323
• Weighted residual factors for significantly intense reflections: 0.0826
• Weighted residual factors for all reflections included in the refinement: 0.0851
• Goodness-of-fit parameter for all reflections included in the refinement: 1.098
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: Yes