Information card for entry 2016921

Structure parameters

• Chemical name: poly[bis(μ~2~-perchlorato-κ^2^<i>O</i>:<i>O</i>')(2,2':6',2''-terpyridine- κ^3^<i>N</i>,<i>N</i>',<i>N</i>'')lead(II)]
• Formula: C15 H11 Cl2 N3 O8 Pb
• Calculated formula: C15 H11 Cl2 N3 O8 Pb
• Title of publication: A new polymorph of poly[bis(μ~2~-perchlorato-κ^2^<i>O</i>:<i>O</i>')(2,2':6',2''-terpyridine-κ^3^<i>N</i>,<i>N</i>',<i>N</i>'')lead(II)] with a greatly extended chain repeat distance
• Authors of publication: Blake, Alexander J.; Caltagirone, Claudia; Lippolis, Vito; Shamsipur, Mojtaba
• Journal of publication: Acta Crystallographica Section C
• Year of publication: 2009
• Journal volume: 65
• Journal issue: 1
• Pages of publication: m33 - m36
• a: 25.44 ± 0.004 Å
• b: 16.333 ± 0.003 Å
• c: 21.916 ± 0.004 Å
• α: 90°
• β: 98.671 ± 0.002°
• γ: 90°
• Cell volume: 9002 ± 3 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 6
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.0935
• Residual factor for significantly intense reflections: 0.0448
• Weighted residual factors for significantly intense reflections: 0.0999
• Weighted residual factors for all reflections included in the refinement: 0.126
• Goodness-of-fit parameter for all reflections included in the refinement: 1.03
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: Yes