Information card for entry 2017048

Structure parameters

• Chemical name: Poly[(<i>N</i>,<i>N</i>-dimethylformamide-κO)(pyrazino[2,3- <i>f</i>][1,10]phenanthroline-κ^2^<i>N</i>^8^,<i>N</i>^9^)(μ~3~-ethylene- 4,4'-dibenzoato-κ^5^O,O':O':O'',O''')lead(II)]
• Formula: C33 H25 N5 O5 Pb
• Calculated formula: C33 H25 N5 O5 Pb
• Title of publication: Poly[(<i>N</i>,<i>N</i>-dimethylformamide-κ<i>O</i>)(μ~3~-4,4'-ethylenedibenzoato-κ^5^<i>O</i>,<i>O</i>':<i>O</i>':<i>O</i>'',<i>O</i>''')(pyrazino[2,3-<i>f</i>][1,10]phenanthroline-κ^2^<i>N</i>^8^,<i>N</i>^9^)lead(II)]
• Authors of publication: Qiao, Qian; Wu, Guo-Qiang; Tang, Tian-Di; Ng, Seik Weng
• Journal of publication: Acta Crystallographica Section C
• Year of publication: 2009
• Journal volume: 65
• Journal issue: 4
• Pages of publication: m146 - m148
• a: 9.0255 ± 0.0007 Å
• b: 25.5628 ± 0.0019 Å
• c: 12.6422 ± 0.0009 Å
• α: 90°
• β: 102.751 ± 0.001°
• γ: 90°
• Cell volume: 2844.8 ± 0.4 ų
• Cell temperature: 295 ± 2 K
• Ambient diffraction temperature: 295 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0549
• Residual factor for significantly intense reflections: 0.0385
• Weighted residual factors for significantly intense reflections: 0.0828
• Weighted residual factors for all reflections included in the refinement: 0.0886
• Goodness-of-fit parameter for all reflections included in the refinement: 1.028
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: Yes