2-Methoxy-3-methyl-6-oxo-4-(2,3,4-tri-<i>O</i>-acetyl-β-<small>D</small>-xylopyranosylamino)-1,6-dihydropyrimidine-5-carbaldehyde 0.065-hydrate and 2-methylsulfanyl-6-oxo-4-(2,3,4-tri-<i>O</i>-acetyl-β-<small>D</small>-xylopyranosylamino)-1,6-dihydropyrimidine-5-carbaldehyde: hydrogen-bonded structures in one or three dimensions
Authors of publication
Cobo, Justo; Nogueras, Manuel; de la Torre, José M.; Glidewell, Christopher
Journal of publication
Acta Crystallographica Section C
Year of publication
2009
Journal volume
65
Journal issue
7
Pages of publication
o321 - o325
a
6.9294 ± 0.0001 Å
b
10.7415 ± 0.0002 Å
c
26.4825 ± 0.0005 Å
α
90°
β
90°
γ
90°
Cell volume
1971.15 ± 0.06 Å3
Cell temperature
120 ± 2 K
Ambient diffraction temperature
120 ± 2 K
Number of distinct elements
5
Space group number
19
Hermann-Mauguin space group symbol
P 21 21 21
Hall space group symbol
P 2ac 2ab
Residual factor for all reflections
0.0432
Residual factor for significantly intense reflections
0.0377
Weighted residual factors for significantly intense reflections
0.0933
Weighted residual factors for all reflections included in the refinement
0.0964
Goodness-of-fit parameter for all reflections included in the refinement
