Conformational and configurational disorder in 6-(3,4,5-trimethoxyphenyl)-6,7-dihydro-5<i>H</i>-1,3-dioxolo[4,5-<i>g</i>]quinolin-8(5<i>H</i>)-one and 6-(1,3-benzodioxol-5-yl)-6,7-dihydro-5<i>H</i>-1,3-dioxolo[4,5-<i>g</i>]quinolin-8-one: a hydrogen-bonded chain of rings and π-stacked hydrogen-bonded chains
Authors of publication
Cuervo, Paola; Abonía, Rodrigo; Cobo, Justo; Glidewell, Christopher
Journal of publication
Acta Crystallographica Section C
Year of publication
2009
Journal volume
65
Journal issue
7
Pages of publication
o326 - o330
a
12.9403 ± 0.0004 Å
b
7.131 ± 0.0002 Å
c
14.7736 ± 0.0007 Å
α
90°
β
103.758 ± 0.0013°
γ
90°
Cell volume
1324.15 ± 0.08 Å3
Cell temperature
120 ± 2 K
Ambient diffraction temperature
120 ± 2 K
Number of distinct elements
4
Space group number
14
Hermann-Mauguin space group symbol
P 1 21/n 1
Hall space group symbol
-P 2yn
Residual factor for all reflections
0.0863
Residual factor for significantly intense reflections
0.0512
Weighted residual factors for significantly intense reflections
0.1136
Weighted residual factors for all reflections included in the refinement
0.1284
Goodness-of-fit parameter for all reflections included in the refinement
