Information card for entry 2017519

Structure parameters

• Chemical name: bis(μ~2~-methylquinolin-8-olato)-κ^3^<i>N</i>,<i>O</i>:<i>O</i>; κ^3^<i>O</i>:<i>N</i>,<i>O</i>-bis[(thiocyanato-κ<i>N</i>)lead(II)]
• Formula: C22 H16 N4 O2 Pb2 S2
• Calculated formula: C22 H16 N4 O2 Pb2 S2
• SMILES: C(=N[Pb]12[n]3c(C)ccc4c3c(ccc4)[O]1[Pb]1([n]3c(ccc4cccc(c34)[O]21)C)N=C=S)=S
• Title of publication: Two polymorphs of a lead(II) complex with 8-hydroxy-2-methylquinoline and thiocyanate
• Authors of publication: Mohammadnezhad, Gholamhossein; Amini, Mostafa M.; Langer, Vratislav
• Journal of publication: Acta Crystallographica Section C
• Year of publication: 2010
• Journal volume: 66
• Journal issue: 2
• Pages of publication: m44 - m47
• a: 7.8556 ± 0.0005 Å
• b: 8.4155 ± 0.0005 Å
• c: 9.155 ± 0.0006 Å
• α: 78.524 ± 0.001°
• β: 69.771 ± 0.001°
• γ: 82.813 ± 0.001°
• Cell volume: 555.5 ± 0.06 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0367
• Residual factor for significantly intense reflections: 0.0303
• Weighted residual factors for significantly intense reflections: 0.0699
• Weighted residual factors for all reflections included in the refinement: 0.0724
• Goodness-of-fit parameter for all reflections included in the refinement: 1.001
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: Yes