A π-stacked chain of hydrogen-bonded dimers in 3-<i>tert</i>-butyl-1-(4-chlorophenyl)-4-phenylindeno[1,2-<i>b</i>]pyrazolo[4,3-<i>e</i>]pyridin-5(1<i>H</i>)-one and a π-stacked sheet of hydrogen-bonded chains in 3-<i>tert</i>-butyl-1-(4-chlorophenyl)-4-(4-methoxyphenyl)indeno[1,2-<i>b</i>]pyrazolo[4,3-<i>e</i>]pyridin-5(1<i>H</i>)-one
Authors of publication
Portilla, Jaime; Lizarazo, Carolina; Cobo, Justo; Glidewell, Christopher
Journal of publication
Acta Crystallographica Section C
Year of publication
2011
Journal volume
67
Journal issue
12
Pages of publication
o479 - o483
a
11.1911 ± 0.0009 Å
b
11.4258 ± 0.0008 Å
c
20.095 ± 0.002 Å
α
97.411 ± 0.006°
β
93.272 ± 0.007°
γ
107.635 ± 0.006°
Cell volume
2415.7 ± 0.4 Å3
Cell temperature
120 ± 2 K
Ambient diffraction temperature
120 ± 2 K
Number of distinct elements
5
Space group number
2
Hermann-Mauguin space group symbol
P -1
Hall space group symbol
-P 1
Residual factor for all reflections
0.0935
Residual factor for significantly intense reflections
0.0484
Weighted residual factors for significantly intense reflections
0.0963
Weighted residual factors for all reflections included in the refinement
0.1152
Goodness-of-fit parameter for all reflections included in the refinement
