Information card for entry 2019305

Structure parameters

• Chemical name: {5,7-Bis[2-(2-methylphenyl)diazen-1-yl]quinolin-8-olato-κ^2^<i>N</i>^1^,<i>O</i>}tricarbonyl(pyridine-κ<i>N</i>)rhenium(I)
• Formula: C31 H23 N6 O4 Re
• Calculated formula: C31 H23 N6 O4 Re
• Title of publication: Distorted octahedral environments in tricarbonylrhenium(I) complexes of 5-[2-(2,4,6-trimethylphenyl)diazen-1-yl]quinolin-8-olate and 5,7-bis[2-(2-methylphenyl)diazen-1-yl]quinolin-8-olate
• Authors of publication: Schutte-Smith, Marietjie; Muller, Theunis J.; Visser, Hendrik G.; Roodt, Andreas
• Journal of publication: Acta Crystallographica Section C
• Year of publication: 2013
• Journal volume: 69
• Journal issue: 12
• Pages of publication: 1467 - 1471
• a: 7.9776 ± 0.0006 Å
• b: 11.6818 ± 0.0008 Å
• c: 15.3994 ± 0.0011 Å
• α: 92.113 ± 0.004°
• β: 98.13 ± 0.003°
• γ: 92.384 ± 0.004°
• Cell volume: 1418.13 ± 0.18 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0286
• Residual factor for significantly intense reflections: 0.0219
• Weighted residual factors for all reflections included in the refinement: 0.0449
• Goodness-of-fit parameter for all reflections included in the refinement: 1.088
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No